In Situ Kinetic Observations on Crystal Nucleation and Growth

J Li, FL Deepak - Chemical reviews, 2022 - ACS Publications
Nucleation and growth are critical steps in crystallization, which plays an important role in
determining crystal structure, size, morphology, and purity. Therefore, understanding the …

Revisiting the growth mechanism of hierarchical semiconductor nanostructures: the role of secondary nucleation in branch formation

L Liu, ML Sushko, EC Buck, X Zhang… - The Journal of …, 2019 - ACS Publications
Although there have been advances in synthesizing hierarchical semiconductor materials,
few studies have investigated the fundamental nucleation mechanisms to explain the origins …

Formation and growth of cerium (III) oxalate nanocrystals by liquid-cell transmission electron microscopy

L Liu, K Kruska, GB Hall, RA Clark, DE Meier, EC Buck - Scripta Materialia, 2022 - Elsevier
Using rare earth elements as analogs for actinide series elements enables studying the
chemistry of these radioactive materials without the inherent risks. A fundamental …

Measurement of Nucleation Rates during Nonclassical Nucleation of Cerium Oxalate: Comparison of Incubation-Quenching and In Situ X-ray Scattering

M Durelle, F Gobeaux, TK Truong… - Crystal Growth & …, 2023 - ACS Publications
There is a growing consensus that numerous crystallization processes occur via a”
nonclassical” mechanism, that is, involve transient noncrystalline structures (molecular …

Continuous morphology-controllable precipitation strategy for europium oxalate hydrates via microchannel reactor

K Tao, H Li, J Cheng, Z Cao, Y Li - Journal of Flow Chemistry, 2023 - Springer
A flow chemistry based continuous morphology-controllable precipitation strategy was
successfully developed for synthesis of europium oxalate hydrate microparticles. The effects …

Integrated atomic force microscopy and x-ray irradiation for in situ characterization of radiation-induced processes

SL Riechers, N Petrik, JS Loring, MK Murphy… - Review of Scientific …, 2021 - pubs.aip.org
Understanding radiation-induced chemical and physical transformations at material
interfaces is important across diverse fields, but experimental approaches are often limited …

Direct visualization of radiation-induced transformations at alkali halide–air interfaces

SL Riechers, NG Petrik, JS Loring… - Communications …, 2021 - nature.com
Radiation driven reactions at mineral/air interfaces are important to the chemistry of the
atmosphere, but experimental constraints (eg simultaneous irradiation, in situ observation …

Unveiling the early stages of the F-element oxalate growth evolution with cryo-TEM

T Meadows, K Kruska, S Tripathi, G Hall… - Microscopy and …, 2020 - cambridge.org
The oxalate anion has long been recognized as an excellent precipitating agent for trivalent
lanthanides and actinides owing to the remarkably low solubility of f-element oxalates in …

Cryo-TEM characterization of the early stages of the uranium oxalate growth evolution

K Kruska, S Tripathi, G Hall, E Buck - Microscopy and Microanalysis, 2021 - cambridge.org
Owing to its curiously low solubility in acidic solutions, the oxalate anion has long been
recognized as an excellent precipitating agent for trivalent lanthanides and actinides [1]. It is …

[PDF][PDF] 254–Unveiling the Early Stages of the F-element Oxalate Growth Evolution with Cryo-TEM

T Meadows, K Kruska, S Tripathi, G Hall, J Carter… - scholar.archive.org
The oxalate anion has long been recognized as an excellent precipitating agent for trivalent
lanthanides and actinides owing to the remarkably low solubility of f-element oxalates in …