Solid-state 13C NMR of carbon nanostructures (milled graphite, graphene, carbon nanotubes, nanodiamonds, fullerenes) in 2000–2019: a mini-review

AS Mazur, MA Vovk, PM Tolstoy - Fullerenes, Nanotubes and …, 2020 - Taylor & Francis
A brief overview is given of the papers published over the last two decades on the subject of
solid-state 13C NMR spectra of such carbon nanostructures as milled graphite and its oxide …

Spectroscopy of light-molecule endofullerenes

MH Levitt - … Transactions of the Royal Society A …, 2013 - royalsocietypublishing.org
Molecular endofullerenes are supramolecular systems consisting of fullerene cages
encapsulating small molecules. Although most early examples consist of encapsulated …

Measurement of sample temperatures under magic-angle spinning from the chemical shift and spin-lattice relaxation rate of 79Br in KBr powder

KR Thurber, R Tycko - Journal of magnetic resonance, 2009 - Elsevier
Accurate determination of sample temperatures in solid state nuclear magnetic resonance
(NMR) with magic-angle spinning (MAS) can be problematic, particularly because frictional …

[图书][B] Chemistry & Physics Of Carbon: Volume 29

LR Radovic - 2004 - taylorfrancis.com
The latest addition to this lauded series, this reference collects pioneering research on the
chemistry and physics of carbon surfaces and the structural properties of carbons. Written by …

Quantum rotation of ortho and para-water encapsulated in a fullerene cage

C Beduz, M Carravetta, JYC Chen… - Proceedings of the …, 2012 - National Acad Sciences
Inelastic neutron scattering, far-infrared spectroscopy, and cryogenic nuclear magnetic
resonance are used to investigate the quantized rotation and ortho–para conversion of …

Biomolecular solid state NMR with magic-angle spinning at 25 K

KR Thurber, R Tycko - Journal of Magnetic Resonance, 2008 - Elsevier
A magic-angle spinning (MAS) probe has been constructed which allows the sample to be
cooled with helium, while the MAS bearing and drive gases are nitrogen. The sample can be …

Helium-cooling and-spinning dynamic nuclear polarization for sensitivity-enhanced solid-state NMR at 14 T and 30 K

Y Matsuki, K Ueda, T Idehara, R Ikeda, I Ogawa… - Journal of Magnetic …, 2012 - Elsevier
We describe a 1H polarization enhancement via dynamic nuclear polarization (DNP) at very
low sample temperature T≈ 30K under magic-angle spinning (MAS) conditions for …

Nuclear spin conversion of water inside fullerene cages detected by low-temperature nuclear magnetic resonance

S Mamone, M Concistrè, E Carignani… - The Journal of …, 2014 - pubs.aip.org
The water-endofullerene H2O@ C60 provides a unique chemical system in which freely
rotating water molecules are confined inside homogeneous and symmetrical carbon cages …

[HTML][HTML] Rotor in a cage: Infrared spectroscopy of an endohedral hydrogen-fullerene complex

S Mamone, M Ge, D Hüvonen, U Nagel… - The Journal of …, 2009 - pubs.aip.org
We report the observation of quantized translational and rotational motion of molecular
hydrogen inside the cages of C 60⁠. Narrow infrared absorption lines at the temperature of …

Symmetry-breaking in the endofullerene H 2 O@ C 60 revealed in the quantum dynamics of ortho and para-water: a neutron scattering investigation

KSK Goh, M Jiménez-Ruiz, MR Johnson… - Physical Chemistry …, 2014 - pubs.rsc.org
Inelastic neutron scattering (INS) has been employed to investigate the quantum dynamics
of water molecules permanently entrapped inside the cages of C60 fullerene molecules …