Solid-state NMR spectroscopy (ssNMR) can provide details about the structure, host–
guest/guest–guest interactions and dynamic behavior of materials at atomic length scales. A …

Oxygen (O), hydrogen (H), carbon (C), and nitrogen (N) are the most common elements
found in organic and biological molecules. Among these four elements, oxygen occupies a …

Solid-state 45Sc NMR spectroscopy, ab initio calculations, and X-ray crystallography are
applied to examine the relationships between 45Sc NMR interactions and molecular …

45Sc NMR isotropic chemical shifts and quadrupole coupling constants of several scandium-
containing solid oxides have been measured. Both parameters prove to be sensitive to local …

We here review the principles and applications of solid‐state NMR spectroscopy of
quadrupolar nuclei, with a special emphasis on structural studies of inorganic solids. Most …

Recently, a pulse scheme for heteronuclear spin decoupling in solid‐state NMR, called
swept‐frequency two‐pulse phase modulation (SWf‐TPPM), was introduced which …

Recent progress in the development and application of signal enhancement methods for
NMR of quadrupolar nuclei in solids is presented. First, various pulse schemes for …

The importance of alkali metal ions (Li+, Na+, K+, Rb+, and Cs+) in chemical and biological
systems is well documented and a vast amount of literature exists [1–8]. The most visible …

Of the several techniques introduced to obtain high-resolution solid-state NMR spectra of
nuclei with half-integer spins larger than one-half the multiple-quantum magic-angle …

The aims of the present study is to describe for the first time the 45Sc MAS NMR spectra of
X2-Sc2SiO5 and C-Sc2Si2O7, to combine the spectroscopic information with the structures …