Photons or electrons? A critical comparison of electrochemistry and photoredox catalysis for organic synthesis

NES Tay, D Lehnherr, T Rovis - Chemical reviews, 2021 - ACS Publications
Redox processes are at the heart of synthetic methods that rely on either electrochemistry or
photoredox catalysis, but how do electrochemistry and photoredox catalysis compare? Both …

Advances in organic electrochemical synthesis

W Zhenhua, M Cong, F Ping, X Haichao… - Acta Chimica …, 2022 - sioc-journal.cn
摘要 有机电化学合成已成为一种实用, 环境友好的合成方法, 广泛应用于氧化,
还原以及氧化还原中性反应. 通过精准调控电流或者电位可在温和反应条件下实现一些具有挑战 …

Catalytic Furfural/5-Hydroxymethyl Furfural Oxidation to Furoic Acid/Furan-2,5-dicarboxylic Acid with H2 Production Using Alkaline Water as the Formal Oxidant

S Kar, QQ Zhou, Y Ben-David… - Journal of the American …, 2022 - ACS Publications
Furfural and 5-hydroxymethyl furfural (HMF) are abundantly available biomass-derived
renewable chemical feedstocks, and their oxidation to furoic acid and furan-2, 5-dicarboxylic …

Autonomous closed-loop mechanistic investigation of molecular electrochemistry via automation

H Sheng, J Sun, O Rodríguez, BB Hoar… - Nature …, 2024 - nature.com
Electrochemical research often requires stringent combinations of experimental parameters
that are demanding to manually locate. Recent advances in automated instrumentation and …

Legion: an instrument for high-throughput electrochemistry

BHR Gerroll, KM Kulesa, CA Ault… - … Measurement Science Au, 2023 - ACS Publications
Electrochemical arrays promise utility for accelerated hypothesis testing and breakthrough
discoveries. Herein, we report a new high-throughput electrochemistry platform, colloquially …

Ni-and Ni/Pd-catalyzed reductive coupling of lignin-derived aromatics to access biobased plasticizers

ZM Su, J Twilton, CB Hoyt, F Wang, L Stanley… - ACS Central …, 2023 - ACS Publications
Lignin-derived aromatic chemicals offer a compelling alternative to petrochemical
feedstocks, and new applications are the focus of extensive interest. 4-Hydroxybenzoic acid …

Identifying opportunities for late-stage CH alkylation with high-throughput experimentation and in silico reaction screening

DF Nippa, K Atz, AT Müller, J Wolfard, C Isert… - Communications …, 2023 - nature.com
Enhancing the properties of advanced drug candidates is aided by the direct incorporation
of specific chemical groups, avoiding the need to construct the entire compound from the …

Emerging reaction technologies in pharmaceutical development: Challenges and opportunities in electrochemistry, photochemistry, and biocatalysis

B Cohen, D Lehnherr, M Sezen-Edmonds… - … Research and Design, 2023 - Elsevier
The challenges and opportunities of developing API manufacturing processes continue to
grow. Molecular complexity of APIs is increasing, process development times are …

Electrosynthesis and Microanalysis in Thin Layer: An Electrochemical Pipette for Rapid Electrolysis and Mechanistic Study of Electrochemical Reactions

BT Punchihewa, V Minda, WG Gutheil… - Angewandte Chemie …, 2023 - Wiley Online Library
Electrochemistry represents unique approaches for the promotion and mechanistic study of
chemical reactions and has garnered increasing attention in different areas of chemistry …

LABS: Laboratory Automation and Batch Scheduling–A Modular Open Source Python Program for the Control of Automated Electrochemical Synthesis with a Web …

MM Hielscher, M Dörr, J Schneider… - Chemistry–An Asian …, 2023 - Wiley Online Library
With LABS, an open source Python‐based lab software is established that enables users to
orchestrate automated synthesis setups. The software consists of a user‐friendly interface …