From angstroms to nanometers: measuring interatomic distances by solid-state NMR

AA Shcherbakov, J Medeiros-Silva, N Tran… - Chemical …, 2021 - ACS Publications
Internuclear distances represent one of the main structural constraints in molecular structure
determination using solid-state NMR spectroscopy, complementing chemical shifts and …

Applications of high-resolution 1H solid-state NMR

SP Brown - Solid State Nuclear Magnetic Resonance, 2012 - Elsevier
This article reviews the large increase in applications of high-resolution 1H magic-angle
spinning (MAS) solid-state NMR, in particular two-dimensional heteronuclear and …

Solid-state NMR molecular snapshots of Aspergillus fumigatus cell wall architecture during a conidial morphotype transition

G Lamon, A Lends, I Valsecchi… - Proceedings of the …, 2023 - National Acad Sciences
While establishing an invasive infection, the dormant conidia of Aspergillus fumigatus transit
through swollen and germinating stages, to form hyphae. During this morphotype transition …

Characterization of different water pools in solid-state NMR protein samples

A Böckmann, C Gardiennet, R Verel… - Journal of biomolecular …, 2009 - Springer
We observed and characterized two distinct signals originating from different pools of water
protons in solid-state NMR protein samples, namely from crystal water which exchanges …

Structure and dynamics of membrane proteins by magic angle spinning solid-state NMR

A McDermott - Annual review of biophysics, 2009 - annualreviews.org
Membrane proteins remain difficult to study by traditional methods. Magic angle spinning
solid-state NMR (MAS SSNMR) methods present an important approach for studying …

The aggregation-enhancing huntingtin N-terminus is helical in amyloid fibrils

VN Sivanandam, M Jayaraman, CL Hoop… - Journal of the …, 2011 - ACS Publications
The 17-residue N-terminus (httNT) directly flanking the polyQ sequence in huntingtin (htt) N-
terminal fragments plays a crucial role in initiating and accelerating the aggregation process …

Water–Polysaccharide Interactions in the Primary Cell Wall of Arabidopsis thaliana from Polarization Transfer Solid-State NMR

PB White, T Wang, YB Park… - Journal of the …, 2014 - ACS Publications
Polysaccharide-rich plant cell walls are hydrated under functional conditions, but the
molecular interactions between water and polysaccharides in the wall have not been …

Structure Calculation from Unambiguous Long-Range Amide and Methyl 1H−1H Distance Restraints for a Microcrystalline Protein with MAS Solid-State NMR …

R Linser, B Bardiaux, V Higman, U Fink… - Journal of the American …, 2011 - ACS Publications
Magic-angle spinning (MAS) solid-state NMR becomes an increasingly important tool for the
determination of structures of membrane proteins and amyloid fibrils. Extensive deuteration …

New applications of solid-state NMR in structural biology

PCA van der Wel - Emerging topics in life sciences, 2018 - portlandpress.com
Various recent developments in solid-state nuclear magnetic resonance (ssNMR)
spectroscopy have enabled an array of new insights regarding the structure, dynamics, and …

Selective methods promote protein solid-state NMR

B Han, J Yang, Z Zhang - The Journal of Physical Chemistry …, 2024 - ACS Publications
Solid-state nuclear magnetic resonance (ssNMR) is indispensable for studying the
structures, dynamics, and interactions of insoluble proteins in native or native-like …