In situ and operando infrared spectroscopy of battery systems: Progress and opportunities

MM Amaral, CG Real, VY Yukuhiro, G Doubek… - Journal of Energy …, 2023 - Elsevier
In situ and operando infrared spectroscopies are powerful techniques to support the design
of novel materials for batteries and the development of new battery systems. These …

Beginner's Guide to Raman Spectroelectrochemistry for Electrocatalysis Study

W Zheng - Chemistry‐Methods, 2023 - Wiley Online Library
The need for continuous observation of electrocatalytic processes under operating
conditions has promoted the popularity of in situ techniques coupled with electrochemical …

Role of Ni in PtNi bimetallic electrocatalysts for hydrogen and value-added chemicals coproduction via glycerol electrooxidation

H Luo, VY Yukuhiro, PS Fernández, J Feng… - ACS …, 2022 - ACS Publications
Pt-based bimetallic electrocatalysts are promising candidates to convert surplus glycerol
from the biodiesel industry to value-added chemicals and coproduce hydrogen. It is …

Highly active Ag/C nanoparticles containing ultra-low quantities of sub-surface Pt for the electrooxidation of glycerol in alkaline media

CC Lima, MVF Rodrigues, AFM Neto, CR Zanata… - Applied Catalysis B …, 2020 - Elsevier
The practical application of Pt-based technologies depends on the lowering in the costs and
one way to face this challenge is by reducing the amount of Pt. Herein, we decorate Ag …

Photoelectrochemical oxidation of glycerol on hematite: thermal effects, in situ FTIR and long-term HPLC product analysis

N Perini, C Hessel, JL Bott-Neto, CT Pires… - Journal of Solid State …, 2021 - Springer
Photoelectrochemical (PEC) oxidation of biomass is a profitable approach to produce
hydrogen by substituting the water oxidation reaction in the electrolyzers' photoanodes …

Direct observation of the CO2 formation and C–H consumption of carbon electrode in an aqueous neutral electrolyte supercapacitor by in-situ FTIR and Raman

MM Amaral, VY Yukuhiro, R Vicentini… - Journal of Energy …, 2022 - Elsevier
Electrical double-layer capacitors (EDLCs) consist of energy storage devices that present
high-power and moderate energy density. The electrolyte and electrode physicochemical …

A portable system for photoelectrochemical detection of lactate on TiO2 nanoparticles and [Ni (salen)] polymeric film

JL Bott-Neto, TS Martins, LA Buscaglia… - Sensors and Actuators B …, 2021 - Elsevier
In this paper we present a portable photoelectrochemical system developed with screen-
printed carbon electrodes (SPCEs) and a 3 W light-emitting diode (LED). The device with 3D …

Development of Electrochemical Cells and Their Application for Spatially Resolved Analysis Using a Multitechnique Approach: From Conventional Experiments to X …

RA Vicente, SP Raju, HVN Gomes, IT Neckel… - Analytical …, 2023 - ACS Publications
Real (electro) catalysts are often heterogeneous, and their activity and selectivity depend on
the properties of specific active sites. Therefore, unveiling the so-called structure–activity …

Electrochemical Glycerol Oxidation on Rhodium Surface: Mechanistic Insights and Catalytic Activity in Alkaline Medium

G Melle, A Rodes, JM Feliu, E Herrero… - ACS …, 2025 - ACS Publications
This study explores the electrochemical properties of rhodium polycrystalline electrodes
applied to the glycerol oxidation reaction (GOR) in an alkaline medium. Our findings …

Judicious selection, validation, and use of reference electrodes for in situ and operando electrocatalysis studies

W Alnoush, R Black, D Higgins - Chem Catalysis, 2021 - cell.com
The development and implementation of in situ and operando characterization techniques to
understand electrocatalytic processes, establish structure-property-performance …