Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …
atomic-resolution structure and dynamics of various chemical, biological, material, and …
1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning
T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …
ago, 1H detection has evolved into the most efficient approach for investigation of …
Solid-state NMR: Methods for biological solids
S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …
transformed from a spectroscopic technique investigating small molecules and industrial …
Automated backbone NMR resonance assignment of large proteins using redundant linking from a single simultaneous acquisition
J Stanek, T Schubeis, P Paluch, P Guntert… - Journal of the …, 2020 - ACS Publications
Thanks to magic-angle spinning (MAS) probes with frequencies of 60–100 kHz, the benefit
of high-sensitivity 1H detection can now be broadly realized in biomolecular solid-state NMR …
of high-sensitivity 1H detection can now be broadly realized in biomolecular solid-state NMR …
Multiplexing experiments in NMR and multi-nuclear MRI
Multiplexing NMR experiments by direct detection of multiple free induction decays (FIDs) in
a single experiment offers a dramatic increase in the spectral information content and often …
a single experiment offers a dramatic increase in the spectral information content and often …
Dipolar Recoupling in Rotating Solids
Magic angle spinning (MAS) nuclear magnetic resonance (NMR) has evolved significantly
over the past three decades and established itself as a vital tool for the structural analysis of …
over the past three decades and established itself as a vital tool for the structural analysis of …
Simultaneous recording of intra-and inter-residue linking experiments for backbone assignments in proteins at MAS frequencies higher than 60 kHz
Obtaining site-specific assignments for the NMR spectra of proteins in the solid state is a
significant bottleneck in deciphering their biophysics. This is primarily due to the time …
significant bottleneck in deciphering their biophysics. This is primarily due to the time …
[HTML][HTML] A suite of solid-state NMR experiments to utilize orphaned magnetization for assignment of proteins using parallel high and low gamma detection
We present a suite of two-receiver solid-state NMR experiments for backbone and side
chain resonance assignment. The experiments rely on either dipolar coupling or scalar …
chain resonance assignment. The experiments rely on either dipolar coupling or scalar …
Taking simultaneous snapshots of intrinsically disordered proteins in action
Intrinsically disordered proteins (IDPs) as well as intrinsically disordered regions (IDRs) of
complex protein machineries have recently been recognized as key players in many cellular …
complex protein machineries have recently been recognized as key players in many cellular …
Exploiting heterogeneous time scale of dynamics to enhance 2D HETCOR solid-state NMR sensitivity
Multidimensional solid-state NMR spectroscopy plays a significant role in offering atomic-
level insights into molecular systems. In particular, heteronuclear chemical shift correlation …
level insights into molecular systems. In particular, heteronuclear chemical shift correlation …