Solid-state 17O NMR studies of organic and biological molecules

G Wu - Progress in Nuclear Magnetic Resonance …, 2008 - Elsevier
Oxygen (O), hydrogen (H), carbon (C), and nitrogen (N) are the most common elements
found in organic and biological molecules. Among these four elements, oxygen occupies a …

Practical aspects of 51V and 93Nb solid-state NMR spectroscopy and applications to oxide materials

OB Lapina, DF Khabibulin, AA Shubin… - Progress in Nuclear …, 2008 - Elsevier
There are many similarities between the first three elements of the Group VB. Two of these
three elements, vanadium and niobium, were discovered in 1801, and Tantalum was …

Influence of the nitric acid treatment on Al removal, framework composition and acidity of BEA zeolite investigated by XRD, FTIR and NMR

R Baran, Y Millot, T Onfroy, JM Krafft… - … and Mesoporous Materials, 2012 - Elsevier
Two different procedures were used to prepare dealuminated BEA zeolite. The first
procedure realized in two steps consisted of first calcination of original tetraethylammonium …

Two kinds of framework Al sites studied in BEA zeolite by X-ray diffraction, Fourier transform infrared spectroscopy, NMR techniques, and V probe

R Hajjar, Y Millot, PP Man, M Che… - The Journal of Physical …, 2008 - ACS Publications
The dealumination of BEA zeolite by treatment with concentrated nitric acid is evidenced by
X-ray diffraction (XRD) and Fourier Transform Infrared (FTIR) spectroscopy. Two …

A brief introduction to the basics of NMR spectroscopy and selected examples of its applications to materials characterization

A Tampieri, M Szabó, F Medina… - Physical Sciences …, 2021 - degruyter.com
Nuclear magnetic resonance (NMR) spectroscopy is an analytical technique that gives
information on the local magnetic field around atomic nuclei. Since the local magnetic field …

Effect of pressure on structure of oxide glasses at high pressure: Insights from solid-state NMR of quadrupolar nuclides

SK Lee - Solid State Nuclear Magnetic Resonance, 2010 - Elsevier
Revealing the structure of oxide glasses at high pressure remains a fundamental yet difficult
problem in modern physical and chemical sciences. The recent advances in solid-state …

Accelerating the acquisition of high-resolution quadrupolar MQ/ST-HETCOR 2D spectra under fast MAS via 1H detection and through-space population transfers

A Sasaki, J Trébosc, JP Amoureux - Journal of Magnetic Resonance, 2021 - Elsevier
Recently, we established an experimental setup protocol to perform the population transfer
from half-integer quadrupolar spin to 1 H nuclei under fast MAS in the context of MQ …

93Nb NMR chemical shift scale for niobia systems

OB Lapina, DF Khabibulin, KV Romanenko… - Solid State Nuclear …, 2005 - Elsevier
93Nb solid-state NMR spectra of a series of inorganic niobates with Nb in different oxygen
coordination environments were measured. For all studied compounds the chemical …

Probing quadrupolar nuclei by solid-state NMR spectroscopy: recent advances

C Fernandez, M Pruski - Solid State NMR, 2012 - Springer
Solid-state nuclear magnetic resonance (NMR) of quadrupolar nuclei has recently
undergone remarkable development of capabilities for obtaining structural and dynamic …

High-resolution heteronuclear correlations between spin-1/2 and half-integer quadrupolar nuclei under fast MAS solid-state NMR

MK Pandey, Y Nishiyama - Biophysical Chemistry, 2024 - Elsevier
High isotropic resolution is essential for the structural elucidation of samples with multiple
sites. In this study, utilizing the benefits of TRAPDOR-based heteronuclear multiple quantum …