Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications

Y Nishiyama, G Hou, V Agarwal, Y Su… - Chemical …, 2022 - ACS Publications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

Facing and overcoming sensitivity challenges in biomolecular NMR spectroscopy

JH Ardenkjaer‐Larsen, GS Boebinger… - Angewandte Chemie …, 2015 - Wiley Online Library
In the Spring of 2013, NMR spectroscopists convened at the Weizmann Institute in Israel to
brainstorm on approaches to improve the sensitivity of NMR experiments, particularly when …

Fast magic-angle sample spinning solid-state NMR at 60–100 kHz for natural abundance samples

Y Nishiyama - Solid State Nuclear Magnetic Resonance, 2016 - Elsevier
In spite of tremendous progress made in pulse sequence designs and sophisticated
hardware developments, methods to improve sensitivity and resolution in solid-state NMR …

Proton-based ultrafast magic angle spinning solid-state NMR spectroscopy

R Zhang, KH Mroue… - Accounts of chemical …, 2017 - ACS Publications
Conspectus Protons are vastly abundant in a wide range of exciting macromolecules and
thus can be a powerful probe to investigate the structure and dynamics at atomic resolution …

Magic angle spinning NMR spectroscopy: a versatile technique for structural and dynamic analysis of solid-phase systems

T Polenova, R Gupta, A Goldbourt - 2015 - ACS Publications
Magic Angle Spinning (MAS) NMR spectroscopy is a powerful method for analysis of a
broad range of systems, including inorganic materials, pharmaceuticals, and …

Interplay of structure and dynamics in functional macromolecular and supramolecular systems as revealed by magnetic resonance spectroscopy

MR Hansen, R Graf, HW Spiess - Chemical Reviews, 2016 - ACS Publications
The characterization of structure and dynamics of macromolecular and supramolecular
systems represents an ongoing challenge. This is due to the fact that soft matter systems …

Multiscale structural control of thiostannate chalcogels with two-dimensional crystalline constituents

TDC Ha, H Lee, YK Kang, K Ahn, HM Jin… - Nature …, 2022 - nature.com
Chalcogenide aerogels (chalcogels) are amorphous structures widely known for their lack of
localized structural control. This study, however, demonstrates a precise multiscale structural …

Structural biology of supramolecular assemblies by magic-angle spinning NMR spectroscopy

CM Quinn, T Polenova - Quarterly reviews of biophysics, 2017 - cambridge.org
In recent years, exciting developments in instrument technology and experimental
methodology have advanced the field of magic-angle spinning (MAS) nuclear magnetic …

Proton-detected solid-state NMR spectroscopy of bone with ultrafast magic angle spinning

KH Mroue, Y Nishiyama, M Kumar Pandey, B Gong… - Scientific reports, 2015 - nature.com
While obtaining high-resolution structural details from bone is highly important to better
understand its mechanical strength and the effects of aging and disease on bone …

Insights into protein misfolding and aggregation enabled by solid-state NMR spectroscopy

PCA van der Wel - Solid state nuclear magnetic resonance, 2017 - Elsevier
The aggregation of proteins and peptides into a variety of insoluble, and often non-native,
aggregated states plays a central role in many devastating diseases. Analogous processes …