Solid phase extraction of trace elements

V Camel - Spectrochimica Acta Part B: Atomic Spectroscopy, 2003 - Elsevier
Conclusion The use of SPE procedures has been growing in the past few years due to their
advantages offered for trace element determinations, namely conservation of species, good …

Electroanalysis with pure, chemically modified and sol‐gel‐derived silica‐based materials

A Walcarius - … An International Journal Devoted to Fundamental …, 2001 - Wiley Online Library
An overview is presented dealing with the use of pure, chemically modified, and sol‐gel‐
derived silicates for designing electrode materials that are then exploited in various …

Chemical modification of silica surface by immobilization of functional groups for extractive concentration of metal ions

PK Jal, S Patel, BK Mishra - Talanta, 2004 - Elsevier
Increased utilization of mechanically stable synthetic matrices particularly silica gel as a
solid support and its surface modification either by impregnation of organic ligands directly …

Silica coated magnetite particles for magnetic removal of Hg2+ from water

PI Girginova, AL Daniel-da-Silva, CB Lopes… - Journal of colloid and …, 2010 - Elsevier
The magnetic removal of Hg2+ from water has been assessed using silica coated magnetite
particles. The magnetite particles were first prepared by hydrolysis of FeSO4 and their …

Solid phase extraction of lead (II), copper (II), cadmium (II) and nickel (II) using gallic acid-modified silica gel prior to determination by flame atomic absorption …

F Xie, X Lin, X Wu, Z Xie - Talanta, 2008 - Elsevier
The immobilization of gallic acid on the surface of amino group-containing silica gel phases
for the formation of a newly chelating matrix (GASG) is described. The newly synthesized …

Synthesis of a novel silica-supported dithiocarbamate adsorbent and its properties for the removal of heavy metal ions

L Bai, H Hu, W Fu, J Wan, X Cheng, L Zhuge… - Journal of Hazardous …, 2011 - Elsevier
Silica-supported dithiocarbamate adsorbent (Si-DTC) was synthesized by anchoring the
chelating agent of macromolecular dithiocarbamate (MDTC) to the chloro-functionalized …

Preparation and characterization of silica gel/chitosan composite for the removal of Cu (II) and Pb (II)

MR Gandhi, S Meenakshi - International Journal of Biological …, 2012 - Elsevier
Silica gel/chitosan composite (SiCS) was prepared via., sol–gel method by mixing silica gel
and chitosan and cross-linked with bifunctional cross-linker glutaraldhyde. The SiCS …

Removal of hexavalent chromium ions using polyaniline/silica gel composite

R Karthik, S Meenakshi - Journal of Water Process Engineering, 2014 - Elsevier
In this study, a composite composed of polyaniline and silica gel was successfully prepared
via in situ polymerization. The prepared polyaniline/silica gel (PANI/SiO 2) composite was …

Selective pre-concentration and solid phase extraction of mercury (II) from natural water by silica gel-loaded dithizone phases

ME Mahmoud, MM Osman, ME Amer - Analytica Chimica Acta, 2000 - Elsevier
Two silica gel phases loaded with dithizone were synthesized based on chemical binding
and physical adsorption approaches. The stability of a chemically modified dithizone phase …

Rate of access to the binding sites in organically modified silicates. 1. Amorphous silica gels grafted with amine or thiol groups

A Walcarius, M Etienne, J Bessière - Chemistry of materials, 2002 - ACS Publications
The speed at which selected reactants are reaching active sites grafted on porous silica gels
of various nature and porosity was evaluated using some model systems: protonation of …