Mechanical, morphological and dielectric properties of sintered mullite ceramics at two different heating rates prepared from alkaline monophasic salts

MMS Sanad, MM Rashad, EA Abdel-Aal… - Ceramics …, 2013 - Elsevier
The sintering behavior of nanocrystalline orthorhombic mullite powders was investigated.
The changes in microstructure, mechanical and dielectric properties with two different …

Formation of mullite from precursor powders: sintering, microstructure and mechanical properties

T Ebadzadeh - Materials Science and Engineering: A, 2003 - Elsevier
The effect of precursor powders using aluminium sulphate/boehmite and colloidal silica on
the green compact, mullitization, densification, microstructure and mechanical properties …

Low temperature pressureless sintering of sol-gel derived mullite

D Amutharani, FD Gnanam - Materials Science and Engineering: A, 1999 - Elsevier
Mullite of stoichiometric composition has been synthesized by sol-gel process. Aluminium
nitrate and ethyl silicate are used as the starting materials to prepare the single phase …

Correlation of the precursor type with densification behavior and microstructure of sintered mullite ceramics

H Ivankovic, E Tkalcec, R Nass, H Schmidt - Journal of the European …, 2003 - Elsevier
The effect of alumina component in diphasic mullite precursors containing alkoxy-derived
silica on the crystallization and sintering behavior of compacts was studied. The phenomena …

Sintering behaviour of precursor mullite powders and resultant microstructures

F Kara, JA Little - Journal of the European Ceramic Society, 1996 - Elsevier
Crystallization and sintering behaviour of two structurally different diphasic precursor mullite
powders were studied. Powder derived from boehmite and colloidal silica formed mullite at …

Novel synthesis of mullite powder with high surface area

M Imose, Y Takano, M Yoshinaka… - Journal of the …, 1998 - Wiley Online Library
Boehmite (AlO (OH)) solid‐solution gel, which yields stoichiometric mullite (3Al2O32SiO2) at
high temperatures, has been prepared by the hydrazine method. The formation process …

Coprecipitation and processing of mullite precursor phases

M Zhou, JMF Ferreira, AT Fonseca… - Journal of the …, 1996 - Wiley Online Library
Ultrafine powders of aluminum‐rich mullite precursor phases were prepared by spraying
mixed acid solutions of silicic acid and aluminum chloride into ammonium hydroxide at …

Transmission Electron Microscopy and Electron Energy‐Loss Spectroscopy Characterization of Glass Phase in Sol‐Gel‐Derived Mullite

HJ Kleebe, G Hilz, G Ziegler - Journal of the American Ceramic …, 1996 - Wiley Online Library
Sol‐gel‐derived mullite ceramics were processed by pressureless sintering at 1600°, 1650°,
and 1700° C for 4 h. Microstructural and microchemical characterization of the mullite …

Synthesis and sintering of pre-mullite powders obtained via carbonate precipitation

S Wang, XQ Shen, HC Yao, ZJ Li - Ceramics International, 2010 - Elsevier
Ultrafine pre-mullite powders, which yield mullite at high temperatures, have been prepared
from colloidal silica and aluminium nitrate via carbonate coprecipitation and followed by …

Effect of composition on the sintering and microstructure of diphasic mullite gels

J Yu, JL Shi, QM Yuan, ZF Yang, YR Chen - Ceramics international, 2000 - Elsevier
Diphasic gels with alumina/silica ratio of 68/32, 71.8/28.2, 74/26, and 76/24 were prepared
and used to study the effect of the precursor composition on the mullite formation process …