Performance parameters for analytical method validation: Controversies and discrepancies among numerous guidelines

F Raposo, C Ibelli-Bianco - TrAC Trends in Analytical Chemistry, 2020 - Elsevier
The main objective of method validation process is to prove that an analytical method is
acceptable for its intended purpose. The necessity for laboratories to use fully validated …

[HTML][HTML] Validation of analytical methods in a pharmaceutical quality system: An overview focused on HPLC methods

BM Marson, V Concentino, AM Junkert, MM Fachi… - Química …, 2020 - SciELO Brasil
Analytical validation has fundamental importance in the scope of Good Manufacturing
Practice (GMP) for pharmaceutical products since it establishes scientific evidence that an …

Ultrasensitive detection of ineradicable and harmful antibiotic chloramphenicol residue in soil, water, and food samples

N Karikalan, A Yamuna, TY Lee - Analytica Chimica Acta, 2023 - Elsevier
Chloramphenicol (CAP) is a harmful antibiotic that inevitably enters our food chain through
natural or manmade means. Its ineradicable residue pollutes soils and water, accumulates …

A comprehensive and critical review of the unstandardized Folin-Ciocalteu assay to determine the total content of polyphenols: The conundrum of the experimental …

F Raposo, R Borja, JA Gutiérrez-González - Talanta, 2024 - Elsevier
Abstract The Folin-Ciocalteu method can be considered to be the most widely used in
laboratories around the world, to quantify the total polyphenols content. Many different …

Dual-emission carbon dots for ratiometric fluorescence sensing of thiabendazole in fruits

S Yang, H Zhu, S Cai, Z Chen, X Liang, Z Li, N Peng… - Talanta, 2024 - Elsevier
Quantitative determination of pesticides in fruits and vegetables is essential for human
healths. Herein, a new dual-emission carbon dots with high fluorescence stability at a pH …

LC-MS/MS Investigation of nitrosamine impurities in certain Sartan group medicinal products available in Istanbul, Türkiye

T Öncü, B Yüksel, E Binay, N Şen - Annales Pharmaceutiques Françaises, 2024 - Elsevier
Nitrosamines (NAs) are molecules that include the nitroso functional group. In 2018, the US
Food and Drug Administration (FDA) received its first report of NAs in pharmaceuticals. The …

A smartphone-assisted paper-based ratio fluorescent probe for the rapid and on-site detection of tetracycline in food samples

J Song, X Liu, X Zhang, J Fan, R Zhang, X Feng - Talanta, 2023 - Elsevier
Rapid, sensitive and portable analytical methods for on-site detection of tetracycline (TC) in
food samples is of critical importance for food safety and public health. In this study, a dual …

Monolithic 3D structural-substrate SERS sensing platform for ultrasensitive and highly-specific analysis of trace bisphenol A

Z Li, Q Xie, J Chi, H Chen, Z Chen, X Lin, G Huang - Talanta, 2024 - Elsevier
Constructing advanced substrates with excellent features is promising for sensitive surface-
enhanced Raman spectroscopy (SERS) detection. Here a novel capillary monolithic 3D …

Digital image-based quantification of chlorpyrifos in water samples using a lipase embedded paper based device

K Sankar, D Lenisha, G Janaki, J Juliana, RS Kumar… - Talanta, 2020 - Elsevier
A paper-based device (PBD) for the detection of chlorpyrifos pesticide at field application
was fabricated based on the principles of enzyme inhibition and image processing …

Quantification of chemicals in non-targeted analysis without analytical standards–Understanding the mechanism of electrospray ionization and making predictions

TA Johnson, DP Abrahamsson - Current Opinion in Environmental Science …, 2024 - Elsevier
The constant creation and release of new chemicals to the environment is forming an ever-
widening gap between available analytical standards and known chemicals. Developing …