Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …
atomic-resolution structure and dynamics of various chemical, biological, material, and …
1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning
T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …
ago, 1H detection has evolved into the most efficient approach for investigation of …
Solid-state NMR: Methods for biological solids
S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …
transformed from a spectroscopic technique investigating small molecules and industrial …
De novo 3D structure determination from sub‐milligram protein samples by solid‐state 100 kHz MAS NMR spectroscopy
Solid‐state NMR spectroscopy is an emerging tool for structural studies of crystalline,
membrane‐associated, sedimented, and fibrillar proteins. A major limitation for many studies …
membrane‐associated, sedimented, and fibrillar proteins. A major limitation for many studies …
Spinning proteins, the faster, the better?
A Böckmann, M Ernst, BH Meier - Journal of Magnetic Resonance, 2015 - Elsevier
Magic-angle spinning (MAS) is a technique that is a prerequisite for high-resolution solid-
state NMR spectroscopy of proteins and other biomolecules. Recently, the 100 kHz limit for …
state NMR spectroscopy of proteins and other biomolecules. Recently, the 100 kHz limit for …
Expanding the horizons for structural analysis of fully protonated protein assemblies by NMR spectroscopy at MAS frequencies above 100 kHz
The recent breakthroughs in NMR probe technologies resulted in the development of MAS
NMR probes with rotation frequencies exceeding 100 kHz. Herein, we explore dramatic …
NMR probes with rotation frequencies exceeding 100 kHz. Herein, we explore dramatic …
Protein resonance assignment at MAS frequencies approaching 100 kHz: a quantitative comparison of J-coupling and dipolar-coupling-based transfer methods
We discuss the optimum experimental conditions to obtain assignment spectra for solid
proteins at magic-angle spinning (MAS) frequencies around 100 kHz. We present a …
proteins at magic-angle spinning (MAS) frequencies around 100 kHz. We present a …
Structure determination of supra-molecular assemblies by solid-state NMR: practical considerations
JP Demers, P Fricke, C Shi, V Chevelkov… - Progress in Nuclear …, 2018 - Elsevier
In the cellular environment, biomolecules assemble in large complexes which can act as
molecular machines. Determining the structure of intact assemblies can reveal …
molecular machines. Determining the structure of intact assemblies can reveal …
Paramagnetic solid-state NMR of materials
M Bertmer - Solid State Nuclear Magnetic Resonance, 2017 - Elsevier
Solid-state NMR (SSNMR) experiments are mainly performed on diamagnetic materials.
However, the study of paramagnetic materials offers access to additional information in …
However, the study of paramagnetic materials offers access to additional information in …
Evolution of CPMAS under fast magic-angle-spinning at 100 kHz and beyond
A Wickramasinghe, S Wang, I Matsuda… - Solid state nuclear …, 2015 - Elsevier
This article describes recent trends of high-field solid-state NMR (SSNMR) experiments for
small organic molecules and biomolecules using 13 C and 15 N CPMAS under ultra-fast …
small organic molecules and biomolecules using 13 C and 15 N CPMAS under ultra-fast …