Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

In spite of tremendous progress made in pulse sequence designs and sophisticated
hardware developments, methods to improve sensitivity and resolution in solid-state NMR …

WURST pulses (wideband, uniform rate, smooth truncation) were first introduced two
decades ago by Kupče and Freeman as a means of achieving broadband adiabatic …

Detecting proton and nitrogen correlations in solid-state nuclear magnetic resonance (NMR)
is important for the structural determination of biological and chemical systems. Recent …

Indirect detection via sensitive spin-1/2 nuclei like protons under magic-angle spinning
(MAS) has been developed to overcome the low spectral sensitivity and resolution of 14 N …

Indirect NMR detection via protons under fast magic-angle spinning can help overcome the
low sensitivity and resolution of low-γ quadrupole nuclei such as 35Cl. A robust and efficient …

14N ultra-wideline (UW), 1H {15N} indirectly-detected HETCOR (idHETCOR) and 15N
dynamic nuclear polarization (DNP) solid-state NMR (SSNMR) experiments, in combination …

Recently, the T-hetero-nuclear multiple quantum coherence (T-HMQC) sequence using the
TRAPDOR (transfer of population in double resonance) recoupling has been introduced for …

A fast magic-angle spinning (MAS, 70 kHz) solid-state NMR experiment is presented that
combines 1H Double-Quantum (DQ) and 14N 1H HMQC (Heteronuclear Multiple …

A novel method to realize rapid repetition of 1 H NMR experiments at ultra-fast MAS
frequencies is demonstrated. The ultra-fast MAS at 110 kHz slows the 1 H–1 H spin …