New sorbents for sample pretreatment: Development and applications

FN Castañeda, DL Prince, SR Peirano… - TrAC Trends in …, 2024 - Elsevier
Sample preparation prior to instrumental analysis is a key step to achieve high quality
qualitative/quantitative analytes determinations present in complex samples. Development …

Ag modified ZnO nanoflowers for the dispersive micro-solid-phase extraction of lead (II) from food and water samples prior to its detection with high-resolution …

O Ozalp, M Soylak - Talanta, 2023 - Elsevier
Ag modified ZnO nanoflowers were synthesized by using hydrothermal method and used as
dispersive micro-solid phase extractant for separation and preconcentration prior to its flame …

Fe3O4-SiO2-MIL-53 (Fe) nanocomposite for magnetic dispersive micro-solid phase extraction of cadmium (II) at trace levels prior to HR-CS-FAAS detection

M Soylak, F Uzcan, O Goktas, ZP Gumus - Food Chemistry, 2023 - Elsevier
A magnetic metal–organic framework Fe 3 O 4-SiO 2-MIL-53 (Fe) nanocomposite was
synthesized for magnetic dispersion micro-solid phase extraction (Md-µSPE) of cadmium in …

Recent advances of sample separation and preconcentration techniques for analytical atomic spectrometry

Q Yang, Y Zhao, H Yu, X Xiong… - Applied Spectroscopy …, 2024 - Taylor & Francis
Analytical atomic spectrometry is a well-established and widely-used analytical technique
for the sensitive detection of inorganic elements in diverse samples. Sample pretreatment …

Tilted fiber Bragg grating surface plasmon resonance based optical fiber cadmium ion trace detection

Z Ren, Z Huang, F Wang, J Wu, J Zhou, Z Wang… - Sensors and Actuators B …, 2023 - Elsevier
A plasmonic tilted fiber Bragg grating (TFBG)-based sensor for the detection of cadmium ion
(Cd 2+) is proposed and demonstrated experimentally. The TFBG is coated with a thin gold …

Cysteine-functionalized selenium nanoparticles for efficient extraction and preconcentration of cadmium, copper, lead, and zinc ions from environmental water …

T Golgoli, K Ghanemi, F Buazar - Journal of Molecular Liquids, 2024 - Elsevier
This study aimed to develop cysteine-functionalized selenium nanoparticles (SeNPs)
supported by γ-alumina (Al 2 O 3@ Se@ Cys) for the effective extraction and …

BaTiO3 is a novel adsorbent for solid-phase extraction of copper at trace levels in food and water samples before HR-CS-FAAS detection

AH Kori, F Uzcan, M Soylak - Journal of Food Composition and Analysis, 2023 - Elsevier
A simple, precise, and rapid method for preconcentration and determination of copper in
food and water samples, based on sonication/vortex-free solid phase extraction with high …

MWCNT@ TiSiO4 nanocomposite for dispersive solid phase extraction of traces cadmium in food and environmental samples

M Soylak, AMA Mohammed, HEH Ahmed - Journal of Food Composition …, 2024 - Elsevier
Cadmium contamination presents substantial hazards to both human health and the
environment due to its persistent presence in ecosystems and toxic characteristics. It …

[HTML][HTML] Determination of high concentration copper ions based on ultraviolet—visible spectroscopy combined with partial least squares regression analysis

Q Liang, L Jiang, J Zheng, N Duan - Processes, 2024 - mdpi.com
With the rapid development of industrialization, the problem of concentration determination
based on the copper production process has been widely concerned, and the accurate …

Separation and Preconcentration of Atrazine on Magnetic Multiwalled Carbon Nanotubes before Determination in Food and Water Samples by High-Performance …

F Uzcan, ZP Gumus, M Soylak - Analytical Letters, 2023 - Taylor & Francis
This work focuses upon the easy and efficient synthesis of multi-walled carbon nanotubes
(MWCNT) decorated with magnetite used in the vortex-assisted magnetic solid-phase …