Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications

Y Nishiyama, G Hou, V Agarwal, Y Su… - Chemical …, 2022 - ACS Publications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

NMR crystallography of molecular organics

P Hodgkinson - Progress in Nuclear Magnetic Resonance …, 2020 - Elsevier
Developments of NMR methodology to characterise the structures of molecular organic
structures are reviewed, concentrating on the previous decade of research in which density …

Structure of fully protonated proteins by proton-detected magic-angle spinning NMR

LB Andreas, K Jaudzems, J Stanek… - Proceedings of the …, 2016 - National Acad Sciences
Protein structure determination by proton-detected magic-angle spinning (MAS) NMR has
focused on highly deuterated samples, in which only a small number of protons are …

Rapid proton-detected NMR assignment for proteins with fast magic angle spinning

E Barbet-Massin, AJ Pell, JS Retel… - Journal of the …, 2014 - ACS Publications
Using a set of six 1H-detected triple-resonance NMR experiments, we establish a method for
sequence-specific backbone resonance assignment of magic angle spinning (MAS) nuclear …

From angstroms to nanometers: measuring interatomic distances by solid-state NMR

AA Shcherbakov, J Medeiros-Silva, N Tran… - Chemical …, 2021 - ACS Publications
Internuclear distances represent one of the main structural constraints in molecular structure
determination using solid-state NMR spectroscopy, complementing chemical shifts and …

Fast magic-angle sample spinning solid-state NMR at 60–100 kHz for natural abundance samples

Y Nishiyama - Solid State Nuclear Magnetic Resonance, 2016 - Elsevier
In spite of tremendous progress made in pulse sequence designs and sophisticated
hardware developments, methods to improve sensitivity and resolution in solid-state NMR …

Proton detection of MAS solid-state NMR spectra of half-integer quadrupolar nuclei

A Venkatesh, MP Hanrahan, AJ Rossini - Solid State Nuclear Magnetic …, 2017 - Elsevier
Fast magic angle spinning (MAS) and proton detection has found widespread application to
enhance the sensitivity of solid-state NMR experiments with spin-1/2 nuclei such as 13 C, 15 …

Probing a hydrogen‐π interaction involving a trapped water molecule in the solid state

E Bartalucci, AA Malär, A Mehnert… - Angewandte Chemie …, 2023 - Wiley Online Library
The detection and characterization of trapped water molecules in chemical entities and
biomacromolecules remains a challenging task for solid materials. We herein present proton …

Nature of Terminating Hydroxyl Groups and Intercalating Water in Ti3C2Tx MXenes: A Study by 1H Solid-State NMR and DFT Calculations

T Kobayashi, Y Sun, K Prenger, D Jiang… - The Journal of …, 2020 - ACS Publications
Since the discovery of two-dimensional transition metal carbides, referred to as MXenes,
research efforts have targeted their applications in energy storage, as lithium-ion batteries …

Proton-detected solid-state NMR spectroscopy of bone with ultrafast magic angle spinning

KH Mroue, Y Nishiyama, M Kumar Pandey, B Gong… - Scientific reports, 2015 - nature.com
While obtaining high-resolution structural details from bone is highly important to better
understand its mechanical strength and the effects of aging and disease on bone …