Uncertainty of results in routine qualitative analysis

A Pulido, I Ruisánchez, R Boqué, FX Rius - TrAC Trends in Analytical …, 2003 - Elsevier
Uncertainty is a performance characteristic that should be estimated in both quantitative and
qualitative results in order to improve knowledge of their reliability. Contrary to quantitative …

Uncertainty of measurement and conformity assessment: a review

E Desimoni, B Brunetti - Analytical and Bioanalytical Chemistry, 2011 - Springer
The uncertainty of measurement is the key indicator of the quality of any experimental result.
Proper consideration of this uncertainty is imperative when testing a sample against …

Determination of Ochratoxin A in wine at sub ng/mL levels by solid-phase microextraction coupled to liquid chromatography with fluorescence detection

A Aresta, R Vatinno, F Palmisano… - … of Chromatography A, 2006 - Elsevier
Solid-phase microextraction (SPME), using a polydimethylsiloxane/divinylbenzene
(PDMS/DVB) fiber, interfaced with liquid chromatography–fluorescence detection (LC–FD) …

Determination of ochratoxin A in pig tissues by liquid–liquid extraction and clean-up and high-performance liquid chromatography

L Monaci, G Tantillo, F Palmisano - Analytical and Bioanalytical Chemistry, 2004 - Springer
A fast, simple, and sensitive HPLC–FD method is described for determination of ochratoxin
A (OTA) in pig kidney and muscle; a small mass (< 2.5 g) of sample and a relatively small …

Fitting straight lines with replicated observations by linear regression: Part II. Testing for homogeneity of variances

A Sayago, AG Asuero - Critical reviews in analytical chemistry, 2004 - Taylor & Francis
The purpose of the previous, this, and subsequent articles in the series is to deal with the
fitting of a straight line to experimental data in those cases in which replicate observations …

Fitting straight lines with replicated observations by linear regression. III. Weighting data

AG Asuero, G González - Critical Reviews in Analytical Chemistry, 2007 - Taylor & Francis
The purpose of this article is to stress the importance of weighting in fitting straight lines with
replicated observations. Nevertheless, single response data are also taken into account …

Ochratoxin A determination in beer by solid-phase microextraction coupled to liquid chromatography with fluorescence detection: A fast and sensitive method for …

A Aresta, F Palmisano, R Vatinno… - Journal of agricultural …, 2006 - ACS Publications
A solid-phase microextraction-liquid chromatography-fluorescence detection (SPME− LC−
FD) method for the determination of ochratoxin A (OTA) in commercial beer samples was …

Uncertainty of qualitative chemical analysis: General methodology and binary test methods

BL Mil'man, LA Konopel'ko - Journal of Analytical Chemistry, 2004 - Springer
Some general problems of qualitative chemical analysis are considered. In particular, the
context of its development is outlined, the concept of hypothesis testing as a basis for the …

Неопределенность результатов качественного химического анализа. Общие положения и бинарные тест-методы

БЛ Мильман, ЛА Конопелько - Журнал аналитической химии, 2004 - elibrary.ru
Рассмотрены общие вопросы качественного химического анализа: контекст его
развития, проверка гипотез как принцип обнаружения и идентификации химических …

Considering uncertainty of measurement when assessing compliance or non-compliance with reference values given in compositional specifications and statutory …

E Desimoni, B Brunetti - Accreditation and Quality Assurance, 2006 - Springer
Considering the uncertainty of measurement (UOM) is mandatory when assessing
compliance with reference values given in compositional specifications and statutory limits …