[HTML][HTML] Sample preparation for geochemical analysis: Strategies and significance

V Balaram, KSV Subramanyam - Advances in Sample Preparation, 2022 - Elsevier
Accurate determination of elemental and isotopic compositions of geological samples must
be a pre-requisite for successful mineral exploration, basic geochemical and …

Recent advances in sample preparation methods for elemental and isotopic analysis of geological samples

W Zhang, Z Hu - Spectrochimica Acta Part B: Atomic Spectroscopy, 2019 - Elsevier
Abstract Knowledge of the elemental compositions and isotopic ratios of geological samples
is a prerequisite for geochemical research. For whole-rock elemental composition and …

Rapid and Complete Digestion of Refractory Geological Samples Using Ultrafine Powder for Accurate Analyses of Trace Elements

YH Liu, S Guo, WJ Li, DS Xue, CF Li… - Analytical Chemistry, 2024 - ACS Publications
Complete sample digestion is a prerequisite for acquiring high-quality analytical results for
geological samples. Closed-vessel acid digestion (bomb) has typically been used for the …

Substituting HF by HBF 4–an optimized digestion method for multi-elemental sediment analysis via ICP-MS/MS

T Zimmermann, M von Der Au, A Reese, O Klein… - Analytical …, 2020 - pubs.rsc.org
Determination of elemental mass fractions in sediments plays a major role in evaluating the
environmental status of aquatic ecosystems. Herewith, the optimization of a new total …

Elemental concentrations of natural graphite and steelmaking slag: development of microwave-assisted acid digestion

V Rantala, M Kokko, R Suvela, M Manninen… - Analytical …, 2024 - Taylor & Francis
To develop more sustainable purification and recovery processes, it is critical to accurately
determine inorganic impurities of natural graphite (NG) and valuable elements present in …

Decomposition of diverse solid inorganic matrices with molten ammonium bifluoride salt for constituent elemental analysis

MJ O'Hara, CM Kellogg, CM Parker, SS Morrison… - Chemical …, 2017 - Elsevier
Abstract Ammonium bifluoride (ABF, NH 4 F· HF) is a well-known reagent for converting
metal oxides to fluorides and for its applications in breaking down minerals and ores in order …

Evaluation of the digestion capability of ammonium bifluoride for the determination of major and trace elements in Ti-rich minerals by ICP-MS

H Liu, Z Hu, T He, W Zhang, K Zong, T Luo… - Journal of Analytical …, 2023 - pubs.rsc.org
Complete sample digestion is a prerequisite to achieve accurate and precise results of
elemental concentrations and isotopic compositions in Ti-rich minerals of interest, such as …

A flux‐free fusion technique for rapid determination of major and trace elements in silicate rocks by LA‐ICP‐MS

Z He, F Huang, H Yu, Y Xiao, F Wang… - Geostandards and …, 2016 - Wiley Online Library
A simple flux‐free fusion technique was developed to analyse major and trace element
compositions of silicate rocks. The sample powders were melted in a molybdenum capsule …

Fabrication and properties of amorphous silica particles by fluorination of zircon using ammonium bifluoride

Y Wang, Y Zhang, G Liang, X Zhao - Journal of Fluorine Chemistry, 2020 - Elsevier
A method to prepare amorphous silica particles from zircon has been developed using the
fluorination method through a three-step process: the fluorination of zircon using ammonium …

Assessment of dissolution of silicate rock reference materials with ammonium bifluoride and nitric acid in a microwave oven

TT Magaldi, MS Navarro… - Geostandards and …, 2019 - Wiley Online Library
The complete dissolution of representative test portions of powdered rock samples for the
determination of the mass fractions of trace elements by ICP‐MS relies either on aggressive …