Determination of the electronic and structural configuration of coordination compounds by synchrotron-radiation techniques

C Garino, E Borfecchia, R Gobetto… - Coordination Chemistry …, 2014 - Elsevier
In this review we provide an overview of the potential of synchrotron radiation techniques to
understand the structural and electronic properties of coordination compounds. Besides the …

Modern X-ray diffraction methods in mineralogy and geosciences

B Lavina, P Dera, RT Downs - Reviews in Mineralogy …, 2014 - pubs.geoscienceworld.org
A century has passed since the first X-ray diffraction experiment (Friedrich et al. 1912).
During this time, X-ray diffraction has become a commonly used technique for the …

[HTML][HTML] The crystalline sponge method updated

M Hoshino, A Khutia, H Xing, Y Inokuma, M Fujita - IUCrJ, 2016 - scripts.iucr.org
Crystalline sponges are porous metal complexes that can absorb and orient common
organic molecules in their pores and make them observable by conventional X-ray structure …

[图书][B] Symmetry relationships between crystal structures: applications of crystallographic group theory in crystal chemistry

U Müller - 2013 - books.google.com
In crystal chemistry and crystal physics, the relations between the symmetry groups (space
groups) of crystalline solids are of special importance. Part 1 of this book presents the …

Crystalline and magnetic structure–property relationship in spinel ferrite nanoparticles

HL Andersen, M Saura-Múzquiz, C Granados-Miralles… - Nanoscale, 2018 - pubs.rsc.org
Magnetic spinel ferrite MFe2O4 (M= Mn, Co, Ni, Zn) nanoparticles have been prepared via
simple, green and scalable hydrothermal synthesis pathways utilizing sub-and supercritical …

Separating electrophilicity and Lewis acidity: The synthesis, characterization, and electrochemistry of the electron deficient tris (aryl) boranes B (C6F5) 3–n (C6Cl5) n …

AE Ashley, TJ Herrington, GG Wildgoose… - Journal of the …, 2011 - ACS Publications
A new family of electron-deficient tris (aryl) boranes, B (C6F5) 3–n (C6Cl5) n (n= 1–3), has
been synthesized, permitting an investigation into the steric and electronic effects resulting …

Crystal melting by light: X-ray crystal structure analysis of an azo crystal showing photoinduced crystal-melt transition

M Hoshino, E Uchida, Y Norikane… - Journal of the …, 2014 - ACS Publications
Trans–cis photoisomerization in an azo compound containing azobenzene chromophores
and long alkyl chains leads to a photoinduced crystal-melt transition (PCMT). X-ray structure …

Structure analysis from powder diffraction data: Rietveld refinement in excel

JSO Evans, IR Evans - Journal of Chemical Education, 2020 - ACS Publications
Powder diffraction is one of the most widely used analytical techniques for characterizing
solid state materials. It can be used for phase or polymorph identification, quantitative …

[HTML][HTML] Water: new aspect of hydrogen bonding in the solid state

MR Milovanović, IM Stanković, JM Živković… - IUCrJ, 2022 - scripts.iucr.org
All water–water contacts in the crystal structures from the Cambridge Structural Database
with dOO≤ 4.0 Å have been found. These contacts were analysed on the basis of their …

Two-step reaction mechanism of roasting spodumene with potassium sulfate

T Ncube, H Oskierski, G Senanayake… - Inorganic …, 2021 - ACS Publications
The conventional process of lithium extraction from α-spodumene (LiAlSi2O6) is energy-
intensive and associated with high byproduct management cost. Here, we investigate an …