Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications

Y Nishiyama, G Hou, V Agarwal, Y Su… - Chemical …, 2022 - ACS Publications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning

T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …

Solid-state NMR dipolar and chemical shift anisotropy recoupling techniques for structural and dynamical studies in biological systems

L Liang, Y Ji, K Chen, P Gao, Z Zhao, G Hou - Chemical Reviews, 2022 - ACS Publications
With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …

Fast magic-angle sample spinning solid-state NMR at 60–100 kHz for natural abundance samples

Y Nishiyama - Solid State Nuclear Magnetic Resonance, 2016 - Elsevier
In spite of tremendous progress made in pulse sequence designs and sophisticated
hardware developments, methods to improve sensitivity and resolution in solid-state NMR …

Proton-based ultrafast magic angle spinning solid-state NMR spectroscopy

R Zhang, KH Mroue… - Accounts of chemical …, 2017 - ACS Publications
Conspectus Protons are vastly abundant in a wide range of exciting macromolecules and
thus can be a powerful probe to investigate the structure and dynamics at atomic resolution …

Understanding surface and interfacial chemistry in functional nanomaterials via solid‐state NMR

A Marchetti, J Chen, Z Pang, S Li, D Ling… - Advanced …, 2017 - Wiley Online Library
Surface and interfacial chemistry is of fundamental importance in functional nanomaterials
applied in catalysis, energy storage and conversion, medicine, and other nanotechnologies …

Using Abundant 1H Polarization to Enhance the Sensitivity of Solid-State NMR Spectroscopy

Z Yan, P Zhao, X Yan, R Zhang - The Journal of Physical …, 2024 - ACS Publications
Solid-state NMR spectroscopy has been playing a significant role in elucidating the
structures and dynamics of materials and proteins at the atomic level for decades. As an …

Three-dimensional NMR spectroscopy of fluorinated pharmaceutical solids under ultrafast magic angle spinning

X Lu, D Skomski, KC Thompson, MJ McNevin… - Analytical …, 2019 - ACS Publications
High-resolution solid-state analysis of multicomponent molecular systems, eg,
pharmaceutical formulations, is a great challenge. Solid-state nuclear magnetic resonance …

Measurement of proton chemical shift anisotropy in solid-state NMR spectroscopy

L Liang, G Hou, X Bao - Solid State Nuclear Magnetic Resonance, 2018 - Elsevier
Proton chemical shift anisotropy (CSA) is significantly important as it provides the
information of the dynamics and local environmental structure of the proton. The …

Proton-detected 3D 1H anisotropic/14N/1H isotropic chemical shifts correlation NMR under fast magic angle spinning on solid samples without isotopic enrichment

MK Pandey, JT Damron, A Ramamoorthy… - Solid State Nuclear …, 2019 - Elsevier
The chemical shift anisotropy (CSA) interaction of a nucleus is an important indicator of the
local electronic environment particularly for the contributions arising from hydrogen (H) …