Sample preparation with solid phase microextraction and exhaustive extraction approaches: Comparison for challenging cases

E Boyacı, Á Rodríguez-Lafuente, K Gorynski… - Analytica chimica …, 2015 - Elsevier
In chemical analysis, sample preparation is frequently considered the bottleneck of the
entire analytical method. The success of the final method strongly depends on …

Electrospray ionization source geometry for mass spectrometry: past, present, and future

I Manisali, DDY Chen, BB Schneider - TrAC Trends in Analytical Chemistry, 2006 - Elsevier
The geometry of an electrospray ion source plays important roles in the processes of analyte
desolvation, ionization, transportation, and detection in a mass spectrometer. We provide a …

Compound-specific, quantitative characterization of organic fluorochemicals in biological matrices

KJ Hansen, LA Clemen, ME Ellefson… - … science & technology, 2001 - ACS Publications
Since the early 1980s, there has been a steady increase in the use of nonvolatile fluorinated
organic compounds for a variety of industrial and commercial applications. The industrial …

Monitoring natural and synthetic estrogens at activated sludge sewage treatment plants and in a receiving river water

C Baronti, R Curini, G D'Ascenzo… - … science & technology, 2000 - ACS Publications
Sewage treatment plant (STP) effluents with primarily domestic inputs are strongly
suspected to be an important source of natural and synthetic estrogens contaminating the …

Matrix effect-free analytical methods for determination of perfluorinated carboxylic acids in environmental matrixes

CR Powley, SW George, TW Ryan… - Analytical chemistry, 2005 - ACS Publications
Perfluorocarboxylic acids (PFCAs) are persistent chemicals that have been found widely in
the environment. Their accurate determination in environmental matrixes, particularly soil …

Ionization and transmission efficiency in an electrospray ionization—mass spectrometry interface

JS Page, RT Kelly, K Tang, RD Smith - Journal of the American Society for …, 2007 - Springer
The ionization and transmission efficiencies of an electrospray ionization (ESI) interface
were investigated to advance the understanding of how these factors affect mass …

Dispersive solid-phase extraction followed by dispersive liquid–liquid microextraction for the determination of some sulfonylurea herbicides in soil by high …

Q Wu, C Wang, Z Liu, C Wu, X Zeng, J Wen… - … of Chromatography A, 2009 - Elsevier
Dispersive solid-phase extraction (DSPE) combined with dispersive liquid–liquid
microextraction (DLLME) has been developed as a new approach for the extraction of four …

Analysis of natural and synthetic estrogenic endocrine disruptors in environmental waters using online preconcentration coupled with LC-APPI-MS/MS

L Viglino, K Aboulfadl, M Prévost, S Sauvé - Talanta, 2008 - Elsevier
This paper describes a fully automated online method for solid-phase extraction coupled
with liquid chromatography and tandem mass spectrometry using atmospheric pressure …

Effect of liquid chromatography separation of complex matrices on liquid chromatography–tandem mass spectrometry signal suppression

BK Choi, DM Hercules, AI Gusev - Journal of Chromatography A, 2001 - Elsevier
The effect of liquid chromatography separation on liquid chromatography–tandem mass
spectrometry (LC–MS–MS) signal response for the characterization of low-molecular-mass …

Confirmatory and quantitative analysis of β-lactam antibiotics in bovine kidney tissue by dispersive solid-phase extraction and liquid chromatography− tandem mass …

CK Fagerquist, AR Lightfield, SJ Lehotay - Analytical chemistry, 2005 - ACS Publications
A simple, rapid, rugged, sensitive, and specific method for the confirmation and quantitation
of 10 β-lactam antibiotics in fortified and incurred bovine kidney tissue has been developed …