Elemental characterization of nuclear materials using total reflection X-ray fluorescence spectrometry

S Dhara, NL Misra - TrAC Trends in Analytical Chemistry, 2019 - Elsevier
The present article gives an overview of the current state of applications of Total reflection X-
Ray Fluorescence (TXRF) spectrometry for the analytical characterization of nuclear …

2016 Atomic Spectrometry Update–a review of advances in X-ray fluorescence spectrometry and its applications

M West, AT Ellis, PJ Potts, C Streli, C Vanhoof… - Journal of Analytical …, 2016 - pubs.rsc.org
This review describes advances in the XRF group of techniques published approximately
between April 2015 and March 2016. Fundamental contributions in the instrumentation …

Direct determination of oxidation states of uranium in mixed-valent uranium oxides using total reflection X-ray fluorescence X-ray absorption near-edge spectroscopy

K Sanyal, A Khooha, G Das, MK Tiwari… - Analytical …, 2017 - ACS Publications
Total reflection X-ray fluorescence (TXRF)-based X-ray absorption near-edge spectroscopy
has been used to determine the oxidation state of uranium in mixed-valent U3O8 and U3O7 …

An X-ray fluorescence and machine learning based methodology for the direct non-destructive compositional analysis of (Th 1− x U x) O 2 fuel pellets

B Kanrar, K Sanyal, A Sarkar, RV Pai - Journal of Analytical Atomic …, 2023 - pubs.rsc.org
A highly sensitive analytical method for elemental quantification of U in (Th1− xUx) O2 mixed
oxide (MOX) fuel pellets is extremely necessary for nuclear fuel quality control. It will be an …

Selective micellar extraction of ultratrace levels of uranium in aqueous samples by task specific ionic liquid followed by its detection employing total reflection X-ray …

A Saha, K Sanyal, N Rawat, SB Deb… - Analytical …, 2017 - ACS Publications
A task specific ionic liquid (TSIL) bearing phosphoramidate group, viz., N-propyl (
diphenylphosphoramidate) trimethylammonium bis (trifluoromethanesulfonyl) imide, was …

Atomic spectrometry update—X-ray fluorescence spectrometry

M West, AT Ellis, PJ Potts, C Streli, C Vanhoof… - Journal of Analytical …, 2012 - pubs.rsc.org
This review demonstrates advances in XRF instrumentation, techniques and data
processing algorithms published during the last year. Pixellated detectors and EDXRF …

A green analytical approach for the direct non-destructive compositional analysis of (Th, U) O 2 fuel pellets by the X-Ray Fluorescence technique using single …

B Kanrar, K Sanyal, RV Pai - Journal of Analytical Atomic Spectrometry, 2022 - pubs.rsc.org
(Th, U) O2-based mixed oxide (MOX) fuel is the proposed fuel for advanced heavy water
reactors (AHWRs), which belong to the third stage of the three-stage Indian nuclear power …

Direct assessment of the variations in the intensity ratios of M and L X-ray lines of U in various compounds by total reflection X-ray fluorescence spectrometry

S Dhara - Spectrochimica Acta Part B: Atomic Spectroscopy, 2023 - Elsevier
A systematic study, to assess the variations in the intensity ratios of uranium M and L X-ray
lines, was carried out using Total reflection X-Ray Fluorescence (TXRF) spectrometry. In …

Total Reflection X-ray Fluorescence Spectrometry: A Comprehensive Review of Critical Components, Analytical Benefits and Practical Applications

Y Zhang, J Yuan, T Xu, L Dong, W Ma… - Critical Reviews in …, 2024 - Taylor & Francis
Total reflection X-ray fluorescence spectrometry (TXRF) is a pivotal technique in modern
atomic spectroscopy, distinguished by its capability for multi-element simultaneous …

Trace element determinations in uranium by energy dispersive X-ray fluorescence spectrometry using thin film specimens

K Sanyal, NL Misra - Spectrochimica Acta Part B: Atomic Spectroscopy, 2019 - Elsevier
Thin film specimens on scotch tape base with analyte amounts in ng level have been used
for trace element determinations in Certified Reference Materials (CRMs) of uranium oxides …