Studying dynamics by magic-angle spinning solid-state NMR spectroscopy: Principles and applications to biomolecules

P Schanda, M Ernst - Progress in nuclear magnetic resonance …, 2016 - Elsevier
Magic-angle spinning solid-state NMR spectroscopy is an important technique to study
molecular structure, dynamics and interactions, and is rapidly gaining importance in …

Solid-state NMR dipolar and chemical shift anisotropy recoupling techniques for structural and dynamical studies in biological systems

L Liang, Y Ji, K Chen, P Gao, Z Zhao, G Hou - Chemical Reviews, 2022 - ACS Publications
With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …

Structural biology of supramolecular assemblies by magic-angle spinning NMR spectroscopy

CM Quinn, T Polenova - Quarterly reviews of biophysics, 2017 - cambridge.org
In recent years, exciting developments in instrument technology and experimental
methodology have advanced the field of magic-angle spinning (MAS) nuclear magnetic …

Dipolar Recoupling in Rotating Solids

V Ladizhansky, RS Palani, M Mardini… - Chemical …, 2024 - ACS Publications
Magic angle spinning (MAS) nuclear magnetic resonance (NMR) has evolved significantly
over the past three decades and established itself as a vital tool for the structural analysis of …

Alamethicin supramolecular organization in lipid membranes from 19F solid-state NMR

ES Salnikov, J Raya, M De Zotti, E Zaitseva… - Biophysical …, 2016 - cell.com
Alamethicins (ALMs) are antimicrobial peptides of fungal origin. Their sequences are rich in
hydrophobic amino acids and strongly interact with lipid membranes, where they cause a …

Probing Molecular Packing of Drug Substances in Nanometer Domains in Pharmaceutical Formulations Using 19F Magic Angle Spinning NMR

P Phyo, W Xu, D Frank, T Li, Y Su - The Journal of Physical …, 2022 - ACS Publications
Structural details of molecular packing provide a fundamental understanding of the resulting
material properties of pharmaceutical materials. For example, both the physical stability and …

Recent advances in solid-state nuclear magnetic resonance techniques to quantify biomolecular dynamics

ED Watt, CM Rienstra - Analytical chemistry, 2014 - ACS Publications
The emergence of solid-state nuclear magnetic resonance (SSNMR) techniques over the
past decade has greatly expanded the range of accessible biomolecules amenable to …

Probing the E/K Peptide Coiled-Coil Assembly by Double Electron–Electron Resonance and Circular Dichroism

EA Golysheva, AL Boyle, B Biondi, P Ruzza, A Kros… - Biochemistry, 2020 - ACS Publications
Double electron–electron resonance (DEER, also known as PELDOR) and circular
dichroism (CD) spectroscopies were explored for the purpose of studying the specificity of …

Halogen and hydrogen bond architectures in switchable chains of di-and trihaloimidazoles

M Andrzejewski, J Marciniak, KW Rajewski… - Crystal Growth & …, 2015 - ACS Publications
Halogen bonds have been employed for controlling the structure of NH··· N hydrogen-
bonded chains in halogenated imidazoles; the CH··· halogen contacts stabilize the coplanar …

Detection of slow dynamics by solid‐state NMR: Application to L‐phenylalanine hydrochloride

W Li, AE Mcdermott - Concepts in Magnetic Resonance Part A, 2013 - Wiley Online Library
New methods for probing dynamical properties of biological macromolecules on the
millisecond timescale will enable a better understanding of the structure–function …