Kinetics of cross-polarization in solid-state NMR: a guide for chemists

W Kolodziejski, J Klinowski - Chemical Reviews, 2002 - ACS Publications
Cross-polarization (CP) from abundant spins I to dilute spins S is a double-resonance
technique1 which overcomes two common problems in the NMR of solids. The first stems …

PISEMA solid-state NMR spectroscopy

A Ramamoorthy, Y Wei, DK Lee - Annual reports on NMR spectroscopy, 2004 - Elsevier
Gone are the days when solid-state NMR spectroscopy was considered to be untouchable-
like as it provided unappealing spectral lines due to poor resolution and sensitivity …

Bone mineral: new insights into its chemical composition

S Von Euw, Y Wang, G Laurent, C Drouet… - Scientific reports, 2019 - nature.com
Some compositional and structural features of mature bone mineral particles remain
unclear. They have been described as calcium-deficient and hydroxyl-deficient carbonated …

Two‐dimensional spectroscopy. Application to nuclear magnetic resonance

WP Aue, E Bartholdi, RR Ernst - The Journal of Chemical Physics, 1976 - pubs.aip.org
Spectroscopy in its classical form has been developed to investigate and to identify
molecular systems in their linear approximation. Linearity is a crucial condition for the …

SIMPSON: a general simulation program for solid-state NMR spectroscopy

M Bak, JT Rasmussen, NC Nielsen - Journal of magnetic resonance, 2011 - Elsevier
A computer program for fast and accurate numerical simulation of solid-state NMR
experiments is described. The program is designed to emulate a NMR spectrometer by …

Rotation of molecules and nuclear spin relaxation

A Steigel, HW Spiess, HW Spiess - Dynamic NMR spectroscopy, 1978 - Springer
Nuclear spin relaxation has been developed as a standard method for studying molecular
motions in liquids, solids, polymers, and—to a lesser extent—gases, staring with the …

[PDF][PDF] High-resolution heteronuclear dipolar solid-state NMR spectroscopy

CH Wu, A Ramamoorthy, SJ Opella - Journal of Magnetic Resonance …, 1994 - mit.edu
By combining polarization inversion (I) with flip-flop (2) Lee-Goldburg (3) homonuclear
decoupling on the abundant I spins following spin-lock cross polarization to the dilute S …

Magic-Angle 13C NMR Analysis of Motion in Solid Glassy Polymers

J Schaefer, EO Stejskal, R Buchdahl - Macromolecules, 1977 - ACS Publications
The dipolar-decoupled, natural abundance Fourier transform and cross-polarization 13C
NMR spectra of seven glassy polymers have been obtained at 22.6 MHz, both with and …

[PDF][PDF] Carbon-13 chemical shift anisotropy

WS Veeman - Progress in nuclear magnetic resonance spectroscopy, 1984 - academia.edu
(Received 13 zyxwvutsrqponmlkjihgfedcbaZYXWVUTSRQPONMLKJIHGFEDC Page 1 Progress
in NMR Spectroscopy, Vol. 16, pp. 193-235, 1984. GU79-6565/84%OW+ .50 Printed in Great …

Separated local field spectra in NMR: determination of structure of solids

RK Hester, JL Ackerman, BL Neff, JS Waugh - Physical Review Letters, 1976 - APS
Various techniques of coherent averaging in NMR are applied in time sequence and the
transient signal is doubly Fourier analyzed. The result is a two-dimensional NMR spectrum …