Quid pro flow

A Laybourn, K Robertson, AG Slater - Journal of the American …, 2023 - ACS Publications
How do you get into flow? We trained in flow chemistry during postdoctoral research and are
now applying it in new areas: materials chemistry, crystallization, and supramolecular …

Densified HKUST-1 monoliths as a route to high volumetric and gravimetric hydrogen storage capacity

DG Madden, D O'Nolan, N Rampal… - Journal of the …, 2022 - ACS Publications
We are currently witnessing the dawn of hydrogen (H2) economy, where H2 will soon
become a primary fuel for heating, transportation, and long-distance and long-term energy …

Assessing thermodynamic selectivity of solid-state reactions for the predictive synthesis of inorganic materials

MJ McDermott, BC McBride, CE Regier… - ACS Central …, 2023 - ACS Publications
Synthesis is a major challenge in the discovery of new inorganic materials. Currently, there
is limited theoretical guidance for identifying optimal solid-state synthesis procedures. We …

A graph-based network for predicting chemical reaction pathways in solid-state materials synthesis

MJ McDermott, SS Dwaraknath, KA Persson - Nature communications, 2021 - nature.com
Accelerated inorganic synthesis remains a significant challenge in the search for novel,
functional materials. Many of the principles which enable “synthesis by design” in synthetic …

Relative kinetics of solid-state reactions: the role of architecture in controlling reactivity

GE Kamm, G Huang, SM Vornholt… - Journal of the …, 2022 - ACS Publications
Countless inorganic materials are prepared via high temperature solid-state reaction of
mixtures of reagents powders. Understanding and controlling the phenomena that limit …

Lowering ternary oxide synthesis temperatures by solid-State cometathesis reactions

A Wustrow, G Huang, MJ McDermott… - Chemistry of …, 2021 - ACS Publications
Low-temperature synthesis routes are necessary for selectively synthesizing many
metastable solid-state materials. Here, we identify a cooperative effect that starting materials …

The RAPTR furnace: a rapid heating and cooling sample furnace for in situ X-ray scattering studies of temperature-induced reactions

D Hu, ML Beauvais, BG Mullens… - Journal of Applied …, 2024 - journals.iucr.org
In situ X-ray scattering provides valuable insights into the mechanisms and kinetics of
reactions and structural transformations. For reactions and structural transformations …

Defect-Accommodating Intermediates Yield Selective Low-Temperature Synthesis of YMnO3 Polymorphs

PK Todd, A Wustrow, RD McAuliffe… - Inorganic …, 2020 - ACS Publications
In the synthesis of complex oxides, solid-state metathesis provides low-temperature
reactions where product selectivity can be achieved through simple changes in precursor …

nmfMapping: a cloud-based web application for non-negative matrix factorization of powder diffraction and pair distribution function datasets

Z Thatcher, CH Liu, L Yang, BC McBride… - … A: Foundations and …, 2022 - journals.iucr.org
A cloud-hosted web-based software application, nmfMapping, for carrying out a non-
negative matrix factorization of a set of powder diffraction or atomic pair distribution function …

Resolving single-layer nanosheets as short-lived intermediates in the solution synthesis of FeS

ML Beauvais, PJ Chupas, D O'Nolan… - ACS Materials …, 2021 - ACS Publications
Short-lived reaction intermediates play a critical role in mediating material synthesis. Such
short-lived species often elude characterization because of the mismatch between the time …