Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications

Y Nishiyama, G Hou, V Agarwal, Y Su… - Chemical …, 2022 - ACS Publications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

Fast magic-angle sample spinning solid-state NMR at 60–100 kHz for natural abundance samples

Y Nishiyama - Solid State Nuclear Magnetic Resonance, 2016 - Elsevier
In spite of tremendous progress made in pulse sequence designs and sophisticated
hardware developments, methods to improve sensitivity and resolution in solid-state NMR …

Proton-based ultrafast magic angle spinning solid-state NMR spectroscopy

R Zhang, KH Mroue… - Accounts of chemical …, 2017 - ACS Publications
Conspectus Protons are vastly abundant in a wide range of exciting macromolecules and
thus can be a powerful probe to investigate the structure and dynamics at atomic resolution …

Spinning proteins, the faster, the better?

A Böckmann, M Ernst, BH Meier - Journal of Magnetic Resonance, 2015 - Elsevier
Magic-angle spinning (MAS) is a technique that is a prerequisite for high-resolution solid-
state NMR spectroscopy of proteins and other biomolecules. Recently, the 100 kHz limit for …

High-resolution proton-detected NMR of proteins at very fast MAS

LB Andreas, T Le Marchand, K Jaudzems… - Journal of magnetic …, 2015 - Elsevier
When combined with high-frequency (currently∼ 60 kHz) magic-angle spinning (MAS),
proton detection boosts sensitivity and increases coherence lifetimes, resulting in narrow 1 …

[PDF][PDF] Solid-state NMR and EPR methods for metal ion battery research

C Li, M Shen, B Hu - Acta Phys. Chim. Sin, 2020 - whxb.pku.edu.cn
The rapid development of batteries, especially lithium-ion batteries, has dramatically
changed our daily lives. From portable electronics to electric vehicles and smart grids …

Proton-detected solid-state NMR spectroscopy of bone with ultrafast magic angle spinning

KH Mroue, Y Nishiyama, M Kumar Pandey, B Gong… - Scientific reports, 2015 - nature.com
While obtaining high-resolution structural details from bone is highly important to better
understand its mechanical strength and the effects of aging and disease on bone …

Ultrafast 1H MAS NMR Crystallography for Natural Abundance Pharmaceutical Compounds

J Struppe, CM Quinn, S Sarkar… - Molecular …, 2019 - ACS Publications
Magic angle spinning (MAS) NMR is a powerful method for the study of pharmaceutical
compounds, and probes with spinning frequencies above 100 kHz enable an atomic …

Spontaneous structural transition and crystal formation in minimal supramolecular polymer model

G Fichman, T Guterman, J Damron… - Science …, 2016 - science.org
The association of building blocks into supramolecular polymers allows the fabrication of
diverse functional architectures at the nanoscale. The use of minimal assembly units to …

A brief introduction to the basics of NMR spectroscopy and selected examples of its applications to materials characterization

A Tampieri, M Szabó, F Medina… - Physical Sciences …, 2021 - degruyter.com
Nuclear magnetic resonance (NMR) spectroscopy is an analytical technique that gives
information on the local magnetic field around atomic nuclei. Since the local magnetic field …