Practical dissolution dynamic nuclear polarization

SJ Elliott, Q Stern, M Ceillier, T El Daraï… - Progress in Nuclear …, 2021 - Elsevier
This review article intends to provide insightful advice for dissolution-dynamic nuclear
polarization in the form of a practical handbook. The goal is to aid research groups to …

Hyperpolarization via dissolution dynamic nuclear polarization: new technological and methodological advances

AC Pinon, A Capozzi, JH Ardenkjær-Larsen - … Resonance Materials in …, 2021 - Springer
Dissolution-DNP is a method to boost liquid-state NMR sensitivity by several orders of
magnitude. The technique consists in hyperpolarizing samples by solid-state dynamic …

Nitrogen-15 dynamic nuclear polarization of nicotinamide derivatives in biocompatible solutions

JP Peters, A Brahms, V Janicaud, M Anikeeva… - Science …, 2023 - science.org
Dissolution dynamic nuclear polarization (dDNP) increases the sensitivity of magnetic
resonance imaging by more than 10,000 times, enabling in vivo metabolic imaging to be …

Frémy's salt as a low-persistence hyperpolarization agent: efficient dynamic nuclear polarization plus rapid radical scavenging

M Negroni, E Turhan, T Kress, M Ceillier… - Journal of the …, 2022 - ACS Publications
Nuclear magnetic resonance (NMR) spectroscopy is a key technique for molecular structure
determination in solution. However, due to its low sensitivity, many efforts have been made …

Multi Electron Spin Cluster Enabled Dynamic Nuclear Polarization with Sulfonated BDPA

C Tobar, K Albanese, R Chaklashiya… - The Journal of …, 2023 - ACS Publications
Dynamic nuclear polarization (DNP) can amplify the solid-state nuclear magnetic resonance
(NMR) signal by several orders of magnitude. The mechanism of DNP utilizing α, γ …

[图书][B] Handbook of high field dynamic nuclear polarization

VK Michaelis, RG Griffin, B Corzilius, S Vega - 2019 - books.google.com
Addresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement
in solid-state NMR spectroscopy This comprehensive handbook is a compendium of the …

A multisample 7 T dynamic nuclear polarization polarizer for preclinical hyperpolarized MR

T Cheng, AP Gaunt, I Marco‐Rius… - NMR in …, 2020 - Wiley Online Library
Dynamic nuclear polarization (DNP) provides the opportunity to boost liquid state magnetic
resonance (MR) signals from selected nuclear spins by several orders of magnitude. A …

Gadolinium Effect at High-Magnetic-Field DNP: 70% 13C Polarization of [U-13C] Glucose Using Trityl

A Capozzi, S Patel, WT Wenckebach… - The journal of …, 2019 - ACS Publications
We show that the trityl electron spin resonance (ESR) features, crucial for an efficient
dynamic nuclear polarization (DNP) process, are sample-composition-dependent. Working …

Trityl radicals: synthesis, properties, and applications

VM Tormyshev, EG Bagryanskaya - Russian Chemical Bulletin, 2021 - Springer
Trityl radicals: synthesis, properties, and applications* Page 1 Russian Chemical Bulletin,
International Edition, Vol. 70, No. 12, pp. 2278—2297, December, 2021 2278 Published in …

C–C cross-coupling reactions of trityl radicals: spin density delocalization, exchange coupling, and a spin label

N Fleck, T Hett, J Brode, A Meyer… - The Journal of …, 2019 - ACS Publications
Organic radicals are usually highly reactive and short-lived species. In contrast,
tetrathiatriarylmethyl radicals, the so-called trityl-or TAM-radicals, are stable and do survive …