Solid-state NMR: Methods for biological solids

S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

Five decades of homonuclear dipolar decoupling in solid-state NMR: Status and outlook

KR Mote, V Agarwal, PK Madhu - Progress in nuclear magnetic resonance …, 2016 - Elsevier
It has been slightly more than fifty years since the first homonuclear spin decoupling
scheme, Lee-Goldburg decoupling, was proposed for removing homonuclear dipolar …

On the binding mode and molecular mechanism of enzymatic polyethylene terephthalate degradation

P Falkenstein, Z Zhao, A Di Pede-Mattatelli… - ACS …, 2023 - ACS Publications
Enzymatic degradation of polyethylene terephthlate (PET) by polyester hydrolases is
currently subject to intensive research, as it is considered as a potential eco-friendly …

[HTML][HTML] 1H line width dependence on MAS speed in solid state NMR–Comparison of experiment and simulation

U Sternberg, R Witter, I Kuprov, JM Lamley… - Journal of Magnetic …, 2018 - Elsevier
Recent developments in magic angle spinning (MAS) technology permit spinning
frequencies of≥ 100 kHz. We examine the effect of such fast MAS rates upon nuclear …

Comprehensive multiphase NMR spectroscopy: basic experimental approaches to differentiate phases in heterogeneous samples

D Courtier-Murias, H Farooq, H Masoom… - Journal of Magnetic …, 2012 - Elsevier
Heterogeneous samples, such as soils, sediments, plants, tissues, foods and organisms,
often contain liquid-, gel-and solid-like phases and it is the synergism between these phases …

Recent advances in solid-state NMR spectroscopy of spin I= 1/2 nuclei

A Lesage - Physical Chemistry Chemical Physics, 2009 - pubs.rsc.org
This perspective contains a brief review of some of the most recent developments in solid-
state NMR spectroscopy of spin I= 1/2 nuclei. Over the last few years, methodological …

Spectroscopic studies of structural dynamics induced by heating and hydration: A case of calcium-terephthalate metal–organic framework

M Mazaj, G Mali, M Rangus… - The journal of …, 2013 - ACS Publications
Structural dynamics of Ca (BDC)(DMF)(H2O) with rhombic-shaped channels and 44 net
topology upon heating and hydration were elucidated by using complementary methods of …

Rapid Quantification of Pharmaceuticals via 1H Solid-State NMR Spectroscopy

YTA Wong, RLEG Aspers, M Uusi-Penttilä… - Analytical …, 2022 - ACS Publications
The physicochemical properties of active pharmaceutical ingredients (APIs) can depend on
their solid-state forms. Therefore, characterization of API forms is crucial for upholding the …

Determining relative proton–proton proximities from the build-up of two-dimensional correlation peaks in 1 H double-quantum MAS NMR: insight from multi-spin …

JP Bradley, C Tripon, C Filip, SP Brown - Physical Chemistry Chemical …, 2009 - pubs.rsc.org
The build-up of intensity—as a function of the number, nrcpl, of POST-C7 elements used for
the excitation and reconversion of double-quantum (DQ) coherence (DQC)—is analysed for …

[HTML][HTML] High-resolution 1H NMR of powdered solids by homonuclear dipolar decoupling

FM Paruzzo, L Emsley - Journal of Magnetic Resonance, 2019 - Elsevier
The development of homonuclear dipolar decoupling sequences to obtain high-resolution 1
H NMR spectra from solids has recently celebrated its 50th birthday. Over the years, a series …