Study of the microstructure of amorphous silica nanostructures using high-resolution electron microscopy, electron energy loss spectroscopy, X-ray powder diffraction …

L Khouchaf, K Boulahya, PP Das, S Nicolopoulos… - Materials, 2020 - mdpi.com
Silica has many industrial (ie, glass formers) and scientific applications. The understanding
and prediction of the interesting properties of such materials are dependent on the …

Microstructural evolution of amorphous silica following alkali–silica reaction

A Hamoudi, L Khouchaf, C Depecker, B Revel… - Journal of non …, 2008 - Elsevier
Combining X-ray diffraction, NMR (CP-MAS and 29Si NMR-MAS) and diffuse reflectance
infra-red Fourier transformed spectroscopy (DRIFTS), the local structural changes induced …

Synthetic Opals or Versatile Nanotools—A One-Step Synthesis of Uniform Spherical Silica Particles

M Laskowska, A Karczmarska, M Schabikowski… - International Journal of …, 2023 - mdpi.com
Synthetic opals, a composition of homogeneous silica spheres in the mesoscale size range,
have attracted the attention of scientists due to their favorable chemical and physical …

Structural characterization of alkali-silica reaction gel: An x-ray absorption fine structure study

RJ Prado, F Tiecher, NP Hasparyk… - Cement and Concrete …, 2019 - Elsevier
This paper sets out to acquire information on the atomic structure of the alkali-silica reaction
gel by using the x-ray absorption fine structure (XAFS) technique to improve the …

Characterization of ASR in Concrete by MAS NMR Spectroscopy

A Peyvandi, I Harsini, D Holmes… - Journal of Materials in …, 2016 - ascelibrary.org
Si 29 MAS NMR spectroscopy was employed for the evaluation of the alkali-silica reaction
(ASR) in laboratory and field concrete specimens. A series of NMR data was collected on …

Evidence of depolymerisation of amorphous silica at medium-and short-range order: XANES, NMR and CP-SEM contributions

L Khouchaf, A Hamoudi, P Cordier - Journal of hazardous materials, 2009 - Elsevier
This work reports medium-and short-range order of changes of amorphous silica submitted
to chemical degradation. Structural changes were studied, using X-ray absorption near edge …

Multi-technique and multi-scale approach applied to study the structural behavior of heterogeneous materials: natural SiO2 case

L Khouchaf, J Verstraete - Journal of materials science, 2007 - Springer
A multi-technique and multi-scale approach have been initiated to study the structural
properties of a natural heterogeneous material. This approach has led us to introduce the …

Characterization of heterogeneous SiO2 materials by scanning electron microscope and micro fluorescence XAS techniques

L Khouchaf, F Boinski, MH Tuilier, AM Flank - Nuclear Instruments and …, 2006 - Elsevier
Micro X-ray absorption near edge structure XANES and micro fluorescence experiments
have been carried out using X-ray microbeam from synchrotron radiation source with high …

Microscopical and mechanical evaluation of the durability of SiO2 aggregates

H El Bahraoui, L Khouchaf, AB Fraj - The European Physical Journal …, 2016 - epjap.org
The durability of SiO 2 compounds is closely related to its structural properties. In this work
three natural siliceous aggregates (called G1, G2 and G3) are studied. Improvement of the …

The study of disorder in amorphous silica, alkali-silica reaction gel and fly ash

C Meral - 2012 - escholarship.org
Significant progress was achieved with the application of Rietveld method to characterize
the crystalline, and nanocrystalline phases in portland cement concrete. However, to obtain …