Dipolar recoupling

NC Nielsen, LA Strassø, AB Nielsen - Solid State NMR, 2012 - Springer
Abstract We describe the principles and applications of dipolar recoupling in solid-state
NMR spectroscopy as a means to access information about molecular structure and transfer …

OPTO: Automated Optimization for Solid-State NMR Spectroscopy

CG Borcik, B DeZonia, T Ravula… - Journal of the …, 2025 - ACS Publications
NMR spectroscopy presents boundless opportunities for understanding the structure,
dynamics, and function for a broad range of scientific applications. Solid-state NMR …

Efficient and robust heteronuclear cross-polarization for high-speed-spinning biological solid-state NMR spectroscopy

S Jain, M Bjerring, NC Nielsen - The journal of physical chemistry …, 2012 - ACS Publications
We present a new and highly efficient approach for heteronuclear coherence transfer in
solid-state NMR spectroscopy under high-speed spinning conditions. The so-called …

Utilizing afterglow magnetization from cross-polarization magic-angle-spinning solid-state NMR spectroscopy to obtain simultaneous heteronuclear multidimensional …

JR Banigan, NJ Traaseth - The journal of physical chemistry B, 2012 - ACS Publications
The time required for data acquisition and subsequent spectral assignment are limiting
factors for determining biomolecular structure and dynamics using solid-state NMR …

A comparison of NCO and NCA transfer methods for biological solid-state NMR spectroscopy

NM Loening, M Bjerring, NC Nielsen… - Journal of Magnetic …, 2012 - Elsevier
Three different techniques (adiabatic passage Hartman-Hahn cross-polarization, optimal
control designed pulses, and EXPORT) are compared for transferring 15N magnetization to …

Optimization of band-selective homonuclear dipolar recoupling in solid-state NMR by a numerical phase search

Z Zhang, H Liu, J Deng, R Tycko, J Yang - The Journal of Chemical …, 2019 - pubs.aip.org
Spin polarization transfers among aliphatic 13 C nuclei, especially 13 Cα–13 Cβ transfers,
permit correlations of their nuclear magnetic resonance (NMR) frequencies that are …

Frequency-selective heteronuclear dephasing and selective carbonyl labeling to deconvolute crowded spectra of membrane proteins by magic angle spinning NMR

NJ Traaseth, G Veglia - Journal of Magnetic Resonance, 2011 - Elsevier
We present a new method that combines carbonyl-selective labeling with frequency-
selective heteronuclear recoupling to resolve the spectral overlap of magic angle spinning …

Recoupling in solid state NMR using γ prepared states and phase matching

J Lin, RG Griffin, N Khaneja - Journal of Magnetic Resonance, 2011 - Elsevier
The paper describes two-dimensional solid state NMR experiments that use powdered
dephased antiphase coherence (γ preparation) to encode chemical shifts in the indirect …

Low-power homonuclear dipolar recoupling using supercycled symmetry-based and exponentially-modulated pulse sequences

AB Nielsen, SK Jain, NC Nielsen - Chemical Physics Letters, 2011 - Elsevier
Aimed at performing dipolar recoupling as part of biological solid-state NMR experiments
without using excessively strong rf irradiation, we present a series of low-power supercycled …

Three pulse recoupling and phase jump matching

J Lin, RG Griffin, NC Nielsen, N Khaneja - Journal of Magnetic Resonance, 2016 - Elsevier
The paper describes a family of novel recoupling pulse sequences, called three pulse
recoupling. These pulse sequences can be employed for both homonuclear and …