Pure shift edited NMR methodologies for the extraction of Homo-and heteronuclear couplings with ultra-high resolution

SK Mishra, N Suryaprakash - Progress in Nuclear Magnetic Resonance …, 2023 - Elsevier
The scalar couplings that result in the splitting of the signals in the NMR spectrum arise due
to the interaction of the nuclear spins, whereby the spin polarization is transmitted through …

PSYCHE pure shift NMR spectroscopy

M Foroozandeh, GA Morris… - Chemistry–A European …, 2018 - Wiley Online Library
Broadband homodecoupling techniques in NMR, also known as “pure shift” methods, aim to
enhance spectral resolution by suppressing the effects of homonuclear coupling interactions …

High-resolution methods for the measurement of scalar coupling constants

Y Lin, Q Zeng, L Lin, Z Chen, PB Barker - Progress in Nuclear Magnetic …, 2018 - Elsevier
Scalar couplings provide important information regarding molecular structure and dynamics.
The measurement of scalar coupling constants constitutes a topic of interest and …

Efficient determination of scalar coupling networks by band selective decoupled 2D NMR spectroscopy

H Zhan, C Gao, C Huang, X Lin, Y Huang, Z Chen - Analytica Chimica Acta, 2023 - Elsevier
Scalar (J) couplings constitute one of vital features observed in NMR spectroscopy and
show valuable information for molecular structure elucidation and conformation analysis …

A quarter of a century of SERF: The progress of an NMR pulse sequence and its application

S Berger - Progress in Nuclear Magnetic Resonance …, 2018 - Elsevier
SERF, an NMR pulse sequence for selectively measuring a spin coupling constant without
interference from other couplings, was published by the current author almost 25 years ago …

Current developments in homonuclear and heteronuclear J‐resolved NMR experiments

T Parella - Magnetic Resonance in Chemistry, 2018 - Wiley Online Library
Two‐dimensional J‐resolved (J res) NMR experiments offer a simple, user‐friendly spectral
representation where the information of coupling constants and chemical shifts are …

Simultaneous determination of multiple coupling networks by high-resolution 2D J-edited NMR spectroscopy

H Zhan, C Huang, C Gao, E Lin, Y Huang, Z Chen - Analytica Chimica Acta, 2021 - Elsevier
J coupling constitutes an important NMR parameter for molecular-level composition analysis
and conformation elucidation. Dozens of J-based approaches have been exploited for J …

Extracting Scalar Couplings From Complex 1H NMR Spectra Using a Simple 2D J‐Resolved Sequence

M Mudgil, ND Kurur - Magnetic Resonance in Chemistry, 2024 - Wiley Online Library
Measurement of scalar couplings between protons is a very challenging task because of
complex multiplet patterns and severe overlapping of these multiplets in congested 1D …

Selective homonuclear 2D J-resolved spectroscopy

D Sinnaeve - eMagRes, 2020 - cnrs.hal.science
Selective 2D J-resolved spectroscopy delivers 2D spectra where exclusively homonuclear
couplings to a selected spin feature as doublets along the indirect dimension, facilitating …

PE-SERF: A sensitivity-improved experiment to measure JHH in crowded spectra

C Zhan, Q Zeng, J Chen, Y Lin, Z Chen - Journal of Magnetic Resonance, 2019 - Elsevier
Aiming at facilitating the analysis of molecular structure, the gradient-encoded selective
refocusing methods (G-SERF) and a great number of its variants for measuring proton …