Solid‐state NMR spectroscopic methods in chemistry

DD Laws, HML Bitter, A Jerschow - Angewandte Chemie …, 2002 - Wiley Online Library
Over the last decades, NMR spectroscopy has grown into an indispensable tool for chemical
analysis, structure determination, and the study of dynamics in organic, inorganic, and …

Applications of heteronuclear NMR spectroscopy in biological and medicinal inorganic chemistry

L Ronconi, PJ Sadler - Coordination Chemistry Reviews, 2008 - Elsevier
There is a wide range of potential applications of inorganic compounds, and metal
coordination complexes in particular, in medicine but progress is hampered by a lack of …

[图书][B] Nuclear magnetic resonance studies of interfacial phenomena

VM Gun'ko, VV Turov - 2013 - books.google.com
This book explores important new NMR spectroscopic methods and describes and
compares the application of NMR to a large variety of useful materials with results from other …

Magic angle spinning NMR spectroscopy: a versatile technique for structural and dynamic analysis of solid-phase systems

T Polenova, R Gupta, A Goldbourt - 2015 - ACS Publications
Magic Angle Spinning (MAS) NMR spectroscopy is a powerful method for analysis of a
broad range of systems, including inorganic materials, pharmaceuticals, and …

One hundred fold overall sensitivity enhancements for Silicon-29 NMR spectroscopy of surfaces by dynamic nuclear polarization with CPMG acquisition

AJ Rossini, A Zagdoun, M Lelli, D Gajan, F Rascón… - Chemical …, 2012 - pubs.rsc.org
Dynamic nuclear polarization (DNP) 29Si solid-state NMR spectra of a hybrid mesoporous
silica material impregnated with aqueous biradical solutions have been acquired with cross …

Proton detection of MAS solid-state NMR spectra of half-integer quadrupolar nuclei

A Venkatesh, MP Hanrahan, AJ Rossini - Solid State Nuclear Magnetic …, 2017 - Elsevier
Fast magic angle spinning (MAS) and proton detection has found widespread application to
enhance the sensitivity of solid-state NMR experiments with spin-1/2 nuclei such as 13 C, 15 …

Structural information from quadrupolar nuclei in solid state NMR

SE Ashbrook, MJ Duer - … in Magnetic Resonance Part A: An …, 2006 - Wiley Online Library
Solid‐state NMR has become the method of choice for determining details of molecular‐
level structure in heterogeneous systems. Though spin‐1/2 nuclei still form the core of most …

New methods for the acquisition of ultra-wideline solid-state NMR spectra of spin-1/2 nuclides

AW MacGregor, LA O'Dell, RW Schurko - Journal of Magnetic Resonance, 2011 - Elsevier
The Wideband Uniform Rate Smooth Truncation–Carr–Purcell Meiboom–Gill (WURST–
CPMG) pulse sequence was recently introduced as a new method of acquiring ultra …

Broadband Cross-Polarization to Half-Integer Quadrupolar Nuclei: Wideline Static NMR Spectroscopy

JJ Kimball, AR Altenhof, MJ Jaroszewicz… - The Journal of …, 2023 - ACS Publications
Cross-polarization (CP) is a technique commonly used for the signal enhancement of NMR
spectra; however, applications to quadrupolar nuclei have heretofore been limited due to a …

Structure and bonding in rhodium coordination compounds: a 103 Rh solid-state NMR and relativistic DFT study

ST Holmes, J Schönzart, AB Philips, JJ Kimball… - Chemical …, 2024 - pubs.rsc.org
This study demonstrates the application of 103Rh solid-state NMR (SSNMR) spectroscopy
to inorganic and organometallic coordination compounds, in combination with relativistic …