Solid‐state NMR spectroscopic methods in chemistry

DD Laws, HML Bitter, A Jerschow - Angewandte Chemie …, 2002 - Wiley Online Library
Over the last decades, NMR spectroscopy has grown into an indispensable tool for chemical
analysis, structure determination, and the study of dynamics in organic, inorganic, and …

Natural abundance deuterium NMR spectroscopy: Developments and analytical applications in liquids, liquid crystals and solid phases

P Lesot, J Courtieu - Progress in Nuclear Magnetic Resonance …, 2009 - Elsevier
Since the beginning of NMR spectroscopy, the observation of magnetically active nuclei with
low isotopic natural abundance as a tracer has been a noteworthy and exciting challenge for …

High resolution solid-state NMR: Averaging of second-order effects by means of a double-rotor

A Samoson, E Lippmaa, A Pines - Molecular Physics, 1988 - Taylor & Francis
By means of rotations around two axes inclined at zeros (magic angles) of the l= 2 and l= 4
Legendre polynomials, first-order and second-order NMR broadening can be averaged …

Resolution in 13C NMR of organic solids using high-power proton decoupling and magic-angle sample spinning

DL VanderHart, WL Earl, AN Garroway - Journal of Magnetic Resonance …, 1981 - Elsevier
The 13 C NMR linewidths observed in organic solids by means of high-power proton
decoupling and magic-angle sample spinning are roughly 10 to 100 times broader than …

Lithium and deuterium NMR studies of acid-leached layered lithium manganese oxides

Y Paik, CP Grey, CS Johnson, JS Kim… - Chemistry of …, 2002 - ACS Publications
6Li and 2H MAS NMR in conjunction with X-ray diffraction is used to study the acid leaching
of the layered Mn (IV) compound Li2MnO3 (ie, Li [Li0. 33Mn0. 67] O2). Lithium NMR shows …

[PDF][PDF] Practical aspects of modern routine solid-state multinuclear magnetic resonance spectroscopy: one-dimensional experiments

DL Bryce, GM Bernard, M Gee… - Canadian journal of …, 2001 - researchgate.net
New solid-state NMR (SSNMR) methods and applications continue to blossom such that a
diverse array of physical, chemical, and biological problems are now being addressed using …

Magic angle spinning

ER Andrew - International Reviews in Physical Chemistry, 1981 - Taylor & Francis
Rapid specimen rotation about an axis inclined at the magic angle of 54° 44′ to the
direction of the applied magnetic field can remove many sources of broadening from the …

2H-NMR Spectroscopy of Solids and Liquid Crystals

GL Hoatson, RL Vold - Solid-State NMR III Organic Matter, 1994 - Springer
Abstract Deuteron Magnetic Resonance spectroscopy (2 H-NMR) is an extremely powerful
technique for investigating molecular structure and dynamics. This aticle covers the last five …

Quadrupole effects in the magic‐angle‐spinning spectra of spin‐1/2 nuclei

N Zumbulyadis, PM Henrichs, RH Young - The Journal of Chemical …, 1981 - pubs.aip.org
Magic‐angle spinning fails to eliminate the effect of dipolar coupling on the spectrum of a
spin‐1/2 nucleus (eg, 13C) coupled to a quadrupolar nucleus (eg, 14N). A quantitative …

[HTML][HTML] A 2H magic-angle spinning solid-state NMR characterisation of lipid membranes in intact bacteria

XL Warnet, M Laadhari, AA Arnold, I Marcotte… - … et Biophysica Acta (BBA …, 2016 - Elsevier
This work proposes a new approach to characterize cell membranes in intact cells by 2 H
solid-state nuclear magnetic resonance (NMR) in only a few hours using magic-angle …