A field guide to flow chemistry for synthetic organic chemists

L Capaldo, Z Wen, T Noël - Chemical science, 2023 - pubs.rsc.org
Flow chemistry has unlocked a world of possibilities for the synthetic community, but the idea
that it is a mysterious “black box” needs to go. In this review, we show that several of the …

Technological innovations in photochemistry for organic synthesis: flow chemistry, high-throughput experimentation, scale-up, and photoelectrochemistry

L Buglioni, F Raymenants, A Slattery… - Chemical …, 2021 - ACS Publications
Photoinduced chemical transformations have received in recent years a tremendous amount
of attention, providing a plethora of opportunities to synthetic organic chemists. However …

Scale-up of photochemical reactions: transitioning from lab scale to industrial production

SDA Zondag, D Mazzarella… - Annual Review of …, 2023 - annualreviews.org
In the past two decades, we have witnessed a rapid emergence of new and powerful
photochemical and photocatalytic synthetic methods. Although these methods have been …

Solar photo-oxidation of recalcitrant industrial wastewater: a review

A Tawfik, MG Alalm, HM Awad, M Islam… - Environmental …, 2022 - Springer
Conventional methods to clean wastewater actually lead to incomplete treatments, calling
for advanced technologies to degrade recalcitrant pollutants. Herein we review solar photo …

Scale-up of a heterogeneous photocatalytic degradation using a photochemical rotor–stator spinning disk reactor

A Chaudhuri, SDA Zondag… - … Process Research & …, 2022 - ACS Publications
Many chemical reactions contain heterogeneous reagents, products, byproducts, or
catalysts, making their transposition from batch to continuous-flow processing challenging …

Continuous stirred-tank reactor cascade platform for self-optimization of reactions involving solids

KY Nandiwale, T Hart, AF Zahrt… - Reaction Chemistry & …, 2022 - pubs.rsc.org
Continuous manufacturing of pharmaceuticals and fine chemicals is attractive due to its
small physical footprint, consistent product quality, and demonstrated benefits from safety …

[HTML][HTML] Recent progress on sonochemical production for the synthesis of efficient photocatalysts and the impact of reactor design

P Adamou, E Harkou, S Hafeez, G Manos, A Villa… - Ultrasonics …, 2023 - Elsevier
Sonochemical-assisted synthesis has flourished recently for the design of photocatalysts.
The main power used is ultrasound that allows the nanomaterials shape and size …

Multiphasic Continuous‐Flow Reactors for Handling Gaseous Reagents in Organic Synthesis: Enhancing Efficiency and Safety in Chemical Processes

AAH Laporte, TM Masson, SDA Zondag… - Angewandte …, 2024 - Wiley Online Library
The use of reactive gaseous reagents for the production of active pharmaceutical
ingredients (APIs) remains a scientific challenge due to safety and efficiency limitations. The …

Ultrasound waves at the service of photocatalysis: From sonochemical synthesis to ultrasound-assisted and piezo-enhanced photocatalysis

D Meroni, CL Bianchi - Current Opinion in Green and Sustainable …, 2022 - Elsevier
Sonication induces physical and chemical effects, such as promoting the mass transfer and
active radical formation, that can be harnessed for process intensification in numerous fields …

Ultrasonic emulsification: basic characteristics, cavitation, mechanism, devices and application

C Yao, S Zhao, L Liu, Z Liu, G Chen - Frontiers of Chemical Science and …, 2022 - Springer
Emulsion systems are widely applied in agriculture, food, cosmetic, pharmaceutical and
biomedical industries. Ultrasound has attracted much attention in emulsion preparation …