Reactions of orthophthalaldehyde with nucleophiles

P Zuman - Chemical reviews, 2004 - ACS Publications
Most substituted benzaldehydes (with the exception of o-and p-nitrobenzaldehydes1, 2)
show a limited reactivity to attacks by weak nucleophiles, like water. 3, 4 Introduction of a …

Derivatization and chromatographic behavior of the o-phthaldialdehyde amino acid derivatives obtained with various SH-group-containing additives

I Molnar-Perl - Journal of chromatography A, 2001 - Elsevier
An overview is presented of HPLC methods currently in use to determine amino acids as
their o-phthaldialdyde derivatives in the presence of various SH-group-containing additives …

Simple method to enable the high resolution determination of total free amino acids in soil solutions and soil extracts

DL Jones, AG Owen, JF Farrar - Soil Biology and Biochemistry, 2002 - Elsevier
Amino acids, either in a free or polymeric state, represent a significant addition of N to most
ecosystems and therefore comprise a key pool in the soil nitrogen cycle. The ability of some …

Rapid automated high performance liquid chromatography method for simultaneous determination of amino acids and biogenic amines in wine, fruit and honey

MT Kelly, A Blaise, M Larroque - Journal of chromatography A, 2010 - Elsevier
This paper reports a new, simple, rapid and economical method for routine determination of
24 amino acids and biogenic amines in grapes and wine. No sample clean-up is required …

Dysregulation of the endothelial nitric oxide pathway is associated with airway inflammation in COPD

B Csoma, A Bikov, L Nagy, B Tóth, T Tábi, G Szűcs… - Respiratory …, 2019 - Springer
Background Chronic obstructive pulmonary disease (COPD) is related to endothelial
dysfunction and the impaired generation of nitric oxide (NO) from L-arginine by the …

Simultaneous analysis of amino acids and amines as their o-phthalaldehyde-ethanethiol-9-fluorenylmethyl chloroformate derivatives in cheese by high-performance …

Á Kőrös, ZS Varga, I Molnár-Perl - Journal of Chromatography A, 2008 - Elsevier
A high-performance liquid chromatographic method (HPLC) with combined diode array and
fluorescence detection of amino acids and amines in various cheese samples is described …

New aspects of the simultaneous analysis of amino acids and amines as their o-phthaldialdehyde derivatives by high-performance liquid chromatography: Analysis of …

D Kutlán, I Molnár-Perl - Journal of Chromatography A, 2003 - Elsevier
A new high-performance liquid chromatography method is described for the simultaneous
quantitation of amino acids and amines for 37 compounds (20 amino acids+ 17 amines), as …

Advancement in the derivatizations of the amino groups with the o-phthaldehyde-thiol and with the 9-fluorenylmethyloxycarbonyl chloride reagents

I Molnár-Perl - Journal of Chromatography B, 2011 - Elsevier
An overview is presented on the advancement of the two most frequently used derivatization
protocols applying the o-phthalaldehyde (OPA)-thiol and the fluorenylmethyloxycarbonyl …

Chirality determination of unusual amino acids using precolumn derivatization and liquid chromatography–electrospray ionization mass spectrometry

S Hess, KR Gustafson, DJ Milanowski, E Alvira… - … of chromatography A, 2004 - Elsevier
Unusual amino acids such as β-methoxytyrosine (β-MeOTyr), allo-threonine (allo-Thr) and
allo-isoleucine (allo-Ile) were derivatized with N-α-(2, 4-dinitro-5-fluorophenyl)-l …

Advances in the evaluation of the stability and characteristics of the amino acid and amine derivatives obtained with the o-phthaldialdehyde/3-mercaptopropionic acid …

Y Mengerink, D Kutlán, F Tóth, A Csámpai… - … of Chromatography A, 2002 - Elsevier
The composition of the amino acid and amine derivatives obtained with the o-
phthaldialdehyde (OPA)/3-mercaptopropionic acid (MPA) and with the OPA/N-acetyl-l …