The relationship between the structure and properties of amino acid ionic liquids

P Ossowicz, J Klebeko, B Roman, E Janus… - Molecules, 2019 - mdpi.com
Ionic liquids based on different l-amino acids (glycine, l-valine, l-leucine, l-isoleucine, l-
histidine, l-methionine, l-tyrosine, l-tryptophan, l-arginine, and l-threonine) and different …

Identification and quantification techniques of polymorphic forms-A review

JT Chambi, C Fandaruff, SL Cuffini - Journal of Pharmaceutical and …, 2024 - Elsevier
In the pharmaceutical industry, the unexpected appearance of crystalline forms could impact
the therapeutic efficacy of an Active Pharmaceutical Ingredient (API). For quality control, a …

A model for a solvent-free synthetic organic research laboratory: click-mechanosynthesis and structural characterization of thioureas without bulk solvents

V Štrukil, MD Igrc, L Fábián, M Eckert-Maksić… - Green chemistry, 2012 - pubs.rsc.org
The mechanochemical click coupling of isothiocyanates and amines has been used as a
model reaction to demonstrate that the concept of a solvent-free research laboratory, which …

A to Z of polymorphs related by proton transfer

A Woods-Ryan, CL Doherty, AJ Cruz-Cabeza - CrystEngComm, 2023 - pubs.rsc.org
The occurrence of tautomeric polymorphism in the Cambridge Structural Database (CSD)
was established to be very rare in a previous study by AJ Cruz-Cabeza and CR Groom …

Hydrogen-Atom-Assisted Tautomerization on Solid Surfaces─ The Case Study of Thioacetamide

S Góbi, I Reva, G Ragupathy, R Fausto… - The Journal of …, 2024 - ACS Publications
Amorphous thioacetamide (TA) ice was prepared by deposition on a low-temperature
substrate in an ultrahigh-vacuum simulation chamber, exposing the sample to a beam of …

Using desmotropes, cocrystals, and salts to manipulate reactivity in mechanochemical organic reactions

M Kralj, S Lukin, G Miletić, I Halasz - The Journal of Organic …, 2021 - ACS Publications
Performing reactions in the solid state offers the largely unexplored possibility of influencing
reactivity by manipulating the solid form of the starting reactants. In this work, we explore the …

Salts and co-crystals of gentisic acid with pyridine derivatives: the effect of proton transfer on the crystal packing (and vice versa)

V Stilinovic, B Kaitner - Crystal growth & design, 2012 - ACS Publications
A series of 22 salts and co-crystals of gentisic acid and pyridine derivatives were
synthesized and their crystal structures were studied by X-ray diffraction. The proton transfer …

Supramolecular stabilization of metastable tautomers in solution and the solid state

M Juribašić, N Bregović, V Stilinović… - … A European Journal, 2014 - Wiley Online Library
This work presents a successful application of a recently reported supramolecular strategy
for stabilization of metastable tautomers in cocrystals to monocomponent, non‐heterocyclic …

Photo-and thermoresponsive N-salicylideneaniline derivatives: solid-state studies and structural aspects

ST Hulushe, FP Malan, EC Hosten, KA Lobb… - New Journal of …, 2022 - pubs.rsc.org
N-Salicylideneaniline (SA) and its derivatives are known to possess chromism upon
exposure to external stimuli. Herein, we present mechanochemical synthesis of a series of …

A novel tautomeric polymorph of anhydrous guanine and its reversible water harvesting property

F Chen, Y Ma, Y Wang, L Qi - Crystal Growth & Design, 2018 - ACS Publications
Tautomeric isomerism is very important in DNA/RNA research, especially base-pair
mismatches. However, the tautomeric polymorph of anhydrous guanine (AG) composed of a …